amino>ethanoic acid hydrochloride

Base Information

Chemical Name:amino>ethanoic acid hydrochloride
CAS No.:123642-60-4
Molecular Formula:C₁₂H₁₆N₂O₆*ClH
Molecular Weight:320.73
Hs Code.:

<N-<1-(4',5'-dimethoxy-2'-nitrophenyl)ethyl>amino>ethanoic acid hydrochloride

Synonyms:amino>ethanoic acid hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of amino>ethanoic acid hydrochloride

Chemical Property:

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Technology Process of amino>ethanoic acid hydrochloride

There total 4 articles about amino>ethanoic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 123642-59-1
tert-butyl amino>ethanoate

: 123642-60-4
amino>ethanoic acid hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 40 ℃; for 0.75h;
DOI:10.1021/jo00292a038

Reference yield:

: 4101-32-0
4',5'-dimethoxy-2'-nitroacetophenone

: 123642-60-4
amino>ethanoic acid hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 23.6 percent / NH₄OAc, NaBH₃CN / methanol / 1) r.t, 4 days 2) 60 deg C, 24h

2: 39 percent / N,N,N',N'-tetramethyl-1,8-napthalenediamine / acetonitrile / 15 h / 60 °C

3: 63 percent / 4M HCl / ethyl acetate / 0.75 h / 40 °C

With hydrogenchloride; ammonium acetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium cyanoborohydride; In methanol; ethyl acetate; acetonitrile;
DOI:10.1021/jo00292a038

Reference yield:

: 123642-58-0
<1-(4',5'-dimethoxy-2'-nitrophenyl)ethyl>amine

: 123642-60-4
amino>ethanoic acid hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / N,N,N',N'-tetramethyl-1,8-napthalenediamine / acetonitrile / 15 h / 60 °C

2: 63 percent / 4M HCl / ethyl acetate / 0.75 h / 40 °C

With hydrogenchloride; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In ethyl acetate; acetonitrile;
DOI:10.1021/jo00292a038