phenyl dichlorodithiophosphate

Base Information

• Chemical Name: phenyl dichlorodithiophosphate
• CAS No.: 10258-61-4
• Molecular Formula: C₆H₅Cl₂PS₂
• Molecular Weight: 243.117
• Mol file: 10258-61-4.mol

Synonyms:phenyl dichlorodithiophosphate

Chemical Property of phenyl dichlorodithiophosphate

Chemical Property:

Purity/Quality:

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Technology Process of phenyl dichlorodithiophosphate

There total 6 articles about phenyl dichlorodithiophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

tetrathiophosphoric acid triphenyl ester (3820-71-1) → phenyl dichlorodithiophosphate (10258-61-4)

Guidance literature:

With trichlorothiophosphine; at 180 - 190 ℃; for 6h;

DOI:10.1007/BF02495702

Reference yield:

Dichlor(phenylthio)phosphan (14684-25-4) → phenyl dichlorodithiophosphate (10258-61-4)

Guidance literature:

With sulfur; at 120 ℃; im geschlossenen Rohr;

Reference yield:

thiophenol (108-98-5) → phenyl dichlorodithiophosphate (10258-61-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate, PCl₃ / CH₂Cl₂ / -35 - 20 °C

2: PSCl₃ / Heating

With potassium carbonate; trichlorophosphate; phosphorus trichloride; In dichloromethane;

upstream raw materials:

Dichlor(phenylthio)phosphan

tetrathiophosphoric acid triphenyl ester

thiophenol

Downstream raw materials:

C₂₂H₁₃F₁₂N₂PS₂

C₂₀H₁₃Cl₂F₆N₂PS₂