(3aR,7aR)-1,3-Dibenzyl-2-(dibromo-fluoro-methyl)-octahydro-benzo[1,3,2]diazaphosphole 2-oxide

Base Information

Chemical Name:(3aR,7aR)-1,3-Dibenzyl-2-(dibromo-fluoro-methyl)-octahydro-benzo[1,3,2]diazaphosphole 2-oxide
CAS No.:349655-89-6
Molecular Formula:C₂₁H₂₄Br₂FN₂OP
Molecular Weight:530.215
Hs Code.:

Synonyms:(3aR,7aR)-1,3-Dibenzyl-2-(dibromo-fluoro-methyl)-octahydro-benzo[1,3,2]diazaphosphole 2-oxide

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Chemical Property of (3aR,7aR)-1,3-Dibenzyl-2-(dibromo-fluoro-methyl)-octahydro-benzo[1,3,2]diazaphosphole 2-oxide

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Technology Process of (3aR,7aR)-1,3-Dibenzyl-2-(dibromo-fluoro-methyl)-octahydro-benzo[1,3,2]diazaphosphole 2-oxide

There total 1 articles about (3aR,7aR)-1,3-Dibenzyl-2-(dibromo-fluoro-methyl)-octahydro-benzo[1,3,2]diazaphosphole 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 65838-10-0,135613-88-6,143443-23-6,191480-61-2
(1R,2R)-N,N'-dibenzylcyclohexane-1,2-diamine

: 349656-00-4
Dibromofluoromethylphosphonic dichloride

: 349655-89-6
(3aR,7aR)-1,3-Dibenzyl-2-(dibromo-fluoro-methyl)-octahydro-benzo[1,3,2]diazaphosphole 2-oxide

Guidance literature:: With triethylamine; In toluene; at 25 ℃; for 2h;
DOI:10.1039/b008906k

Reference yield:

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 349655-89-6
(3aR,7aR)-1,3-Dibenzyl-2-(dibromo-fluoro-methyl)-octahydro-benzo[1,3,2]diazaphosphole 2-oxide

: (1S,2R)-2-((3aR,7aR)-1,3-Dibenzyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-2-fluoro-cyclopropanecarboxylic acid tert-butyl ester

: (1R,2R)-2-((3aR,7aR)-1,3-Dibenzyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-2-fluoro-cyclopropanecarboxylic acid tert-butyl ester

: (1S,2S)-2-((3aR,7aR)-1,3-Dibenzyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-2-fluoro-cyclopropanecarboxylic acid tert-butyl ester

: (1R,2S)-2-((3aR,7aR)-1,3-Dibenzyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-2-fluoro-cyclopropanecarboxylic acid tert-butyl ester

Guidance literature:: With tetraethylammonium bromide; magnesium; In N,N-dimethyl-formamide; Electrolysis;
DOI:10.1039/b008906k

Reference yield:

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 349655-89-6
(3aR,7aR)-1,3-Dibenzyl-2-(dibromo-fluoro-methyl)-octahydro-benzo[1,3,2]diazaphosphole 2-oxide

: (1S,2R)-2-((3aR,7aR)-1,3-Dibenzyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-2-fluoro-cyclopropanecarboxylic acid methyl ester

: (1R,2R)-2-((3aR,7aR)-1,3-Dibenzyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-2-fluoro-cyclopropanecarboxylic acid methyl ester

: (1S,2S)-2-((3aR,7aR)-1,3-Dibenzyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-2-fluoro-cyclopropanecarboxylic acid methyl ester

: (1R,2S)-2-((3aR,7aR)-1,3-Dibenzyl-2-oxo-octahydro-2λ⁵-benzo[1,3,2]diazaphosphol-2-yl)-2-fluoro-cyclopropanecarboxylic acid methyl ester

Guidance literature:: With tetraethylammonium bromide; magnesium; In N,N-dimethyl-formamide; Title compound not separated from byproducts.; Electrolysis;
DOI:10.1039/b008906k