(E)-3,5-bis-methoxymethoxy-4-(3-methylbut-2-enyl)-4'-triisopropylsilyloxystilbene

Base Information

Chemical Name:(E)-3,5-bis-methoxymethoxy-4-(3-methylbut-2-enyl)-4'-triisopropylsilyloxystilbene
CAS No.:1269415-98-6
Molecular Formula:C₃₂H₄₈O₅Si
Molecular Weight:540.816
Hs Code.:

Synonyms:(E)-3,5-bis-methoxymethoxy-4-(3-methylbut-2-enyl)-4'-triisopropylsilyloxystilbene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3,5-bis-methoxymethoxy-4-(3-methylbut-2-enyl)-4'-triisopropylsilyloxystilbene

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Technology Process of (E)-3,5-bis-methoxymethoxy-4-(3-methylbut-2-enyl)-4'-triisopropylsilyloxystilbene

There total 3 articles about (E)-3,5-bis-methoxymethoxy-4-(3-methylbut-2-enyl)-4'-triisopropylsilyloxystilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1269415-96-4
(E)-3,5-bis-methoxymethoxy-4'-triisopropylsilyloxystilbene

: 870-63-3
prenyl bromide

: 1269415-98-6
(E)-3,5-bis-methoxymethoxy-4-(3-methylbut-2-enyl)-4'-triisopropylsilyloxystilbene

Guidance literature:: (E)-3,5-bis-methoxymethoxy-4'-triisopropylsilyloxystilbene; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 2h; Inert atmosphere;

prenyl bromide; In tetrahydrofuran; hexane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/np100696f

Reference yield:

: 1269415-94-2
diethyl (4-((triisopropylsilyl)oxy)benzyl)phosphonate

: 1269415-98-6
(E)-3,5-bis-methoxymethoxy-4-(3-methylbut-2-enyl)-4'-triisopropylsilyloxystilbene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; hexane; 1.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/np100696f

Reference yield:

: 76280-61-0
3,5-di-[(methoxymethyl)oxy]benzaldehyde

: 1269415-98-6
(E)-3,5-bis-methoxymethoxy-4-(3-methylbut-2-enyl)-4'-triisopropylsilyloxystilbene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; hexane; 1.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/np100696f