methyl 6-amino>hex-2-enoate

Base Information

• Chemical Name: methyl 6-amino>hex-2-enoate
• CAS No.: 137256-46-3
• Molecular Formula: C₁₈H₂₉NO₂Si
• Molecular Weight: 319.519

Synonyms:methyl 6-amino>hex-2-enoate

Chemical Property of methyl 6-amino>hex-2-enoate

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Technology Process of methyl 6-amino>hex-2-enoate

There total 1 articles about methyl 6-amino>hex-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

4-(Benzyl-trimethylsilanylmethyl-amino)-butyraldehyde; hydrochloride (137256-28-1) + methyl (triphenylphosphoranylidene)acetate (21204-67-1,2605-67-6) → methyl 6-amino>hex-2-enoate (137256-46-3)

Guidance literature:

for 12h; Heating;

Reference yield: 67.0%

methyl 6-amino>hex-2-enoate (137256-46-3) → 1-benzyl-3-(carbomethoxymethyl)piperidine (118299-61-9) + methyl 2-(1-benzylpyrrolidin-2-yl)acetate (118299-62-0)

Guidance literature:

With dichloro-acetic acid; In methanol; acetonitrile; for 1h; Irradiation;

Reference yield: 60.0%

methyl 6-amino>hex-2-enoate (137256-46-3) → methyl 2-(1-benzylpyrrolidin-2-yl)acetate (118299-62-0)

Guidance literature:

In acetonitrile; electrolysis;

DOI:10.1016/S0040-4039(00)73962-1

upstream raw materials:

4-(Benzyl-trimethylsilanylmethyl-amino)-butyraldehyde; hydrochloride

methyl (triphenylphosphoranylidene)acetate

Downstream raw materials:

1-benzyl-3-(carbomethoxymethyl)piperidine

methyl 2-(1-benzylpyrrolidin-2-yl)acetate

{1-[2-(3-Methoxycarbonylmethyl-piperidin-1-yl)-1,2-diphenyl-ethyl]-piperidin-3-yl}-acetic acid methyl ester

{1-[(4-Cyano-phenyl)-phenyl-methyl]-piperidin-3-yl}-acetic acid methyl ester

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