[C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]⁽¹⁺⁾*BF₄^(1-)=[C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]BF₄

Base Information

• Chemical Name: [C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]⁽¹⁺⁾*BF₄^(1-)=[C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]BF₄
• CAS No.: 83201-96-1
• Molecular Formula: BF₄*C₁₉H₁₉NiS₂
• Molecular Weight: 456.986
• Mol file: 83201-96-1.mol

Synonyms:[C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]⁽¹⁺⁾*BF₄^(1-)=[C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]BF₄

Chemical Property of [C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]⁽¹⁺⁾*BF₄^(1-)=[C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]BF₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]⁽¹⁺⁾*BF₄^(1-)=[C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]BF₄

There total 1 articles about [C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]⁽¹⁺⁾*BF₄^(1-)=[C₅H₅Ni(C₆H₅SCH₂CH₂SC₆H₅)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{(π-C5H5)3Ni2}BF4 + 1,2-bis(phenylthio)ethane (622-20-8) → nickelocene (1271-28-9) + [C5H5Ni(C6H5SCH2CH2SC6H5)](1+)*BF4(1-)=[C5H5Ni(C6H5SCH2CH2SC6H5)]BF4 (83201-96-1)

Guidance literature:

In not given; under Ar, large excess of (PhSCH2)2;

DOI:10.1016/S0022-328X(00)85708-3

Reference yield:

[C5H5Ni(C6H5SCH2CH2SC6H5)](1+)*BF4(1-)=[C5H5Ni(C6H5SCH2CH2SC6H5)]BF4 (83201-96-1) → {C5H5Ni(C6H5)2P(CH2)2P(C6H5)2}(1+)*BF4(1-)={C5H5Ni(C6H5)2P(CH2)2P(C6H5)2}BF4

Guidance literature:

With bis-(diphenylphosphino)-ethane; In chloroform; under Ar;

DOI:10.1016/S0022-328X(00)85708-3

upstream raw materials:

1,2-bis(phenylthio)ethane