N-Methyl-morpholine-4-carboximidothioic acid (E)-3-oxo-3-p-tolyl-propenyl ester; hydrochloride

Base Information

Chemical Name:N-Methyl-morpholine-4-carboximidothioic acid (E)-3-oxo-3-p-tolyl-propenyl ester; hydrochloride
CAS No.:83251-56-3
Molecular Formula:C₁₆H₂₀N₂O₂S*ClH
Molecular Weight:340.874
Hs Code.:

Synonyms:N-Methyl-morpholine-4-carboximidothioic acid (E)-3-oxo-3-p-tolyl-propenyl ester; hydrochloride

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Chemical Property of N-Methyl-morpholine-4-carboximidothioic acid (E)-3-oxo-3-p-tolyl-propenyl ester; hydrochloride

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Technology Process of N-Methyl-morpholine-4-carboximidothioic acid (E)-3-oxo-3-p-tolyl-propenyl ester; hydrochloride

There total 1 articles about N-Methyl-morpholine-4-carboximidothioic acid (E)-3-oxo-3-p-tolyl-propenyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2741-03-9
morpholine-4-carbothioic acid methylamide

: 41124-45-2
(E)-3-chloro-1-(4-methylphenyl)-2-propenone

: 83251-56-3
N-Methyl-morpholine-4-carboximidothioic acid (E)-3-oxo-3-p-tolyl-propenyl ester; hydrochloride

Guidance literature:: In acetone;
DOI:10.1016/0040-4020(82)85072-2

Reference yield: 79.0%

: 83251-56-3
N-Methyl-morpholine-4-carboximidothioic acid (E)-3-oxo-3-p-tolyl-propenyl ester; hydrochloride

: 83241-75-2
N-Methyl-morpholine-4-carboximidothioic acid (Z)-3-oxo-3-p-tolyl-propenyl ester

Guidance literature:: With potassium carbonate; In acetone;
DOI:10.1016/0040-4020(82)85072-2

Reference yield:

: 83251-56-3
N-Methyl-morpholine-4-carboximidothioic acid (E)-3-oxo-3-p-tolyl-propenyl ester; hydrochloride

: 83241-92-3
Morpholine-4-carbothioic acid methyl-((E)-3-oxo-3-p-tolyl-propenyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / K₂CO₃ / acetone

2: 100 percent / toluene / 5 h / Heating

With potassium carbonate; In acetone; toluene;
DOI:10.1016/0040-4020(82)85072-2