o-cinnamyloxyacetophenone oxime

Base Information

• Chemical Name: o-cinnamyloxyacetophenone oxime
• CAS No.: 855425-13-7
• Molecular Formula: C₁₇H₁₇NO₂
• Molecular Weight: 267.327
• Mol file: 855425-13-7.mol

Synonyms:o-cinnamyloxyacetophenone oxime

Chemical Property of o-cinnamyloxyacetophenone oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of o-cinnamyloxyacetophenone oxime

There total 1 articles about o-cinnamyloxyacetophenone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(E)-1-[2-(3-phenylprop-2-enyloxy)phenyl]ethanone (321903-41-7) → o-cinnamyloxyacetophenone oxime (855425-13-7)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; Heating;

DOI:10.1139/v05-049

Reference yield: 59.0%

o-cinnamyloxyacetophenone oxime (855425-13-7) → 3-benzyl-5-methyl-2,3-dihydro-benzo[f][1,4]oxazepine-4-oxide + (E)-1-[2-(3-phenylprop-2-enyloxy)phenyl]ethanone (321903-41-7)

Guidance literature:

With silica gel; for 0.25h; microwave irradiation;

DOI:10.1139/v05-049

Reference yield:

o-cinnamyloxyacetophenone oxime (855425-13-7) → (3RS,3aSR,9bRS)-1,9b-dimethyl-3-phenyl-1,3a,4,9b-tetrahydro-3H-chromeno[4,3-c]isoxazole

Guidance literature:

Multi-step reaction with 2 steps

1: 10 percent / silica gel / 0.25 h / microwave irradiation

2: 95 percent / sodium hydrogen carbonate; silica gel / 0.25 h / microwave irradiation

With silica gel; sodium hydrogencarbonate;

DOI:10.1139/v05-049

upstream raw materials:

(E)-1-[2-(3-phenylprop-2-enyloxy)phenyl]ethanone

Downstream raw materials:

(E)-1-[2-(3-phenylprop-2-enyloxy)phenyl]ethanone