allyl 2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl-(1->4)-2,6-di-O-benzoyl-α-D-glucopyranoside

Base Information

Chemical Name:allyl 2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl-(1->4)-2,6-di-O-benzoyl-α-D-glucopyranoside
CAS No.:607364-85-2
Molecular Formula:C₄₉H₄₄O₁₅
Molecular Weight:872.879
Hs Code.:

Synonyms:allyl 2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl-(1->4)-2,6-di-O-benzoyl-α-D-glucopyranoside

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Chemical Property of allyl 2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl-(1->4)-2,6-di-O-benzoyl-α-D-glucopyranoside

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Technology Process of allyl 2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl-(1->4)-2,6-di-O-benzoyl-α-D-glucopyranoside

There total 3 articles about allyl 2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl-(1->4)-2,6-di-O-benzoyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.1%

: 607364-84-1
allyl 2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl-(1->4)-2,6-di-O-benzoyl-3-O-tert-butyldimethylsilyl-α-D-glucopyranoside

: 607364-85-2
allyl 2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl-(1->4)-2,6-di-O-benzoyl-α-D-glucopyranoside

Guidance literature:: With trifluoroacetic acid; In water; at 60 ℃; for 3h;
DOI:10.1081/CAR-120023470

Reference yield:

: 127446-71-3
Allyl 2,6-di-O-benzoyl-α-D-glucopyranoside

: 607364-85-2
allyl 2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl-(1->4)-2,6-di-O-benzoyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / imidazole / dimethylformamide / 4 h / 20 °C

2: 78.4 percent / Me₃SiOTf / CH₂Cl₂ / 1 h / 0 °C

3: 95.1 percent / CF₃CO₂H / H₂O / 3 h / 60 °C

With 1H-imidazole; trimethylsilyl trifluoromethanesulfonate; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1081/CAR-120023470

Reference yield:

: 607364-83-0
allyl 2,6-di-O-benzoyl-3-O-tert-butyldimethylsilyl-α-D-glucopyranoside

: 607364-85-2
allyl 2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl-(1->4)-2,6-di-O-benzoyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 78.4 percent / Me₃SiOTf / CH₂Cl₂ / 1 h / 0 °C

2: 95.1 percent / CF₃CO₂H / H₂O / 3 h / 60 °C

With trimethylsilyl trifluoromethanesulfonate; trifluoroacetic acid; In dichloromethane; water;
DOI:10.1081/CAR-120023470