diethyl (S)-<<2-<(4-morpholinylsulfonyl)amino>-3-phenyl-1-oxopropyl>amino>propanedioate

Base Information

Chemical Name:diethyl (S)-<<2-<(4-morpholinylsulfonyl)amino>-3-phenyl-1-oxopropyl>amino>propanedioate
CAS No.:127953-50-8
Molecular Formula:C₂₀H₂₉N₃O₈S
Molecular Weight:471.532
Hs Code.:

Synonyms:diethyl (S)-<<2-<(4-morpholinylsulfonyl)amino>-3-phenyl-1-oxopropyl>amino>propanedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (S)-<<2-<(4-morpholinylsulfonyl)amino>-3-phenyl-1-oxopropyl>amino>propanedioate

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Technology Process of diethyl (S)-<<2-<(4-morpholinylsulfonyl)amino>-3-phenyl-1-oxopropyl>amino>propanedioate

There total 1 articles about diethyl (S)-<<2-<(4-morpholinylsulfonyl)amino>-3-phenyl-1-oxopropyl>amino>propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.3%

: 13433-00-6
diethyl aminomalonate hydrochloride

: 124278-39-3
N-(4-MorpholinYlsulfonyl)-L-phenylalanine

: 127953-50-8
diethyl (S)-<<2-<(4-morpholinylsulfonyl)amino>-3-phenyl-1-oxopropyl>amino>propanedioate

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; 1.) 0 deg C, 30 min, 2.) RT, overnight;
DOI:10.1021/jm00108a004

Reference yield:

: 127953-50-8
diethyl (S)-<<2-<(4-morpholinylsulfonyl)amino>-3-phenyl-1-oxopropyl>amino>propanedioate

: 127953-52-0,132199-77-0,132293-94-8
6-tert-Butoxycarbonylamino-2-[(S)-2-(morpholine-4-sulfonylamino)-3-phenyl-propionylamino]-hex-4-ynoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH, 2.) KI / 1.) DMSO, 4 h, 2.) 40 h

2: 1.) 2N NaOH / 1.) dioxane, ethanol, RT, overnight, 2.) toluene, dioxane, reflux, 3 h

With sodium hydroxide; sodium hydride; potassium iodide;
DOI:10.1021/jm00108a004

Reference yield:

: 77369-60-9
(4-chlorobut-2-ynyl)carbamic Acid Tert-Butyl Ester

: 127953-50-8
diethyl (S)-<<2-<(4-morpholinylsulfonyl)amino>-3-phenyl-1-oxopropyl>amino>propanedioate

: 127953-51-9
diethyl (S)-2-<4-<<(1,1-dimethylethoxy)carbonyl>amino>-2-butynyl>-2-<<2-<(4-morpholinylsulfonyl)amino>-1-oxo-3-phenylpropyl>amino>propanedioate

Guidance literature:: With sodium hydride; potassium iodide; Yield given. Multistep reaction; 1.) DMSO, 4 h, 2.) 40 h;
DOI:10.1021/jm00108a004