2-((5-((2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yl)oxy)pentyl)(2-((2-mercaptoethyl)amino)ethyl)amino)ethanethiol

Base Information

Chemical Name:2-((5-((2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yl)oxy)pentyl)(2-((2-mercaptoethyl)amino)ethyl)amino)ethanethiol
CAS No.:1384435-30-6
Molecular Formula:C₂₆H₃₈N₄O₂S₂
Molecular Weight:502.745
Hs Code.:

Synonyms:2-((5-((2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yl)oxy)pentyl)(2-((2-mercaptoethyl)amino)ethyl)amino)ethanethiol

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Chemical Property of 2-((5-((2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yl)oxy)pentyl)(2-((2-mercaptoethyl)amino)ethyl)amino)ethanethiol

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Technology Process of 2-((5-((2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yl)oxy)pentyl)(2-((2-mercaptoethyl)amino)ethyl)amino)ethanethiol

There total 7 articles about 2-((5-((2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yl)oxy)pentyl)(2-((2-mercaptoethyl)amino)ethyl)amino)ethanethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₄H₆₆N₄O₂S₂

: 1384435-30-6
2-((5-((2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yl)oxy)pentyl)(2-((2-mercaptoethyl)amino)ethyl)amino)ethanethiol

Guidance literature:: With triethylsilane; at 0 ℃; for 0.166667h;
DOI:10.1016/j.bmcl.2012.05.010

Reference yield:

: 1383563-18-5
2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-ol

: 1384435-30-6
2-((5-((2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yl)oxy)pentyl)(2-((2-mercaptoethyl)amino)ethyl)amino)ethanethiol

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 90 °C

2: potassium carbonate / acetonitrile / 90 °C

3: trifluoroacetic acid / 0.17 h / 20 °C

4: triethylsilane / 0.17 h / 0 °C

With triethylsilane; potassium carbonate; trifluoroacetic acid; In acetonitrile;
DOI:10.1016/j.bmcl.2012.05.010

Reference yield:

: 1383563-17-4
4-(5-methoxybenzo[d]oxazol-2-yl)-N,N-dimethylbenzenamine

: 1384435-30-6
2-((5-((2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yl)oxy)pentyl)(2-((2-mercaptoethyl)amino)ethyl)amino)ethanethiol

Guidance literature:: Multi-step reaction with 5 steps

1: boron tribromide / dichloromethane / 3 h / -78 °C

2: potassium carbonate / acetonitrile / 90 °C

3: potassium carbonate / acetonitrile / 90 °C

4: trifluoroacetic acid / 0.17 h / 20 °C

5: triethylsilane / 0.17 h / 0 °C

With triethylsilane; boron tribromide; potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2012.05.010