Technology Process of C23H24FNO6S
There total 3 articles about C23H24FNO6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C26H30FNO6S;
With
boron trichloride;
In
dichloromethane;
at -30 - -20 ℃;
for 0.5h;
With
water;
In
dichloromethane;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 2 h / 20 °C
2.1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 80 °C
4.1: boron trichloride / dichloromethane / 0.5 h / -30 - -20 °C
4.2: Cooling with ice
With
hydrogen; boron trichloride; potassium carbonate; triethylamine;
palladium 10% on activated carbon;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 80 °C
3.1: boron trichloride / dichloromethane / 0.5 h / -30 - -20 °C
3.2: Cooling with ice
With
boron trichloride; potassium carbonate; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;