acetyltricarbonyl(methyldiphenylphosphine)cobalt(I)

Base Information

Chemical Name:acetyltricarbonyl(methyldiphenylphosphine)cobalt(I)
CAS No.:86177-65-3
Molecular Formula:C₁₈H₁₆CoO₄P
Molecular Weight:386.29
Hs Code.:

Synonyms:acetyltricarbonyl(methyldiphenylphosphine)cobalt(I)

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Chemical Property of acetyltricarbonyl(methyldiphenylphosphine)cobalt(I)

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Technology Process of acetyltricarbonyl(methyldiphenylphosphine)cobalt(I)

There total 2 articles about acetyltricarbonyl(methyldiphenylphosphine)cobalt(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 86196-53-4
tricarbonylmethyl(methyldiphenylphosphine)cobalt(I)

: 86177-65-3
acetyltricarbonyl(methyldiphenylphosphine)cobalt(I)

Guidance literature:: With carbon monoxide; In tetrahydrofuran; 1 atm CO, 2 h; chromy. (N2-atmosphere);

Reference yield:

: Co₂*6CO*2P(C₆H₅)2(CH₃) = {Co(CO)3(P(C₆H₅)2(CH₃))}2

: 86177-65-3
acetyltricarbonyl(methyldiphenylphosphine)cobalt(I)

Guidance literature:: With sodium amalgam; carbon monoxide; methyl iodide; In tetrahydrofuran; Co complex was stirred with sodium amalgam in THF for 5 h, amalgam was removed, MeI was added, soln. was stirred for 2 h as CO was bubbled through it; evapn., extn. with Et2O, concn., hexane adding; elem. anal.;
DOI:10.1021/om50003a002