C₁₇H₂₇IO₄Si

Base Information

Chemical Name:C₁₇H₂₇IO₄Si
CAS No.:1622094-35-2
Molecular Formula:C₁₇H₂₇IO₄Si
Molecular Weight:450.389
Hs Code.:

C<sub>17</sub>H<sub>27</sub>IO<sub>4</sub>Si

Synonyms:C₁₇H₂₇IO₄Si

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Chemical Property of C₁₇H₂₇IO₄Si

Chemical Property:

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Technology Process of C₁₇H₂₇IO₄Si

There total 4 articles about C₁₇H₂₇IO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1622094-21-6
C₁₇H₂₇IO₃Si

: 1622094-35-2
C₁₇H₂₇IO₄Si

Guidance literature:: With tert.-butylhydroperoxide; copper dichloride; In water; acetonitrile; at 20 - 50 ℃; for 16h;
DOI:10.1002/chem.201402323

Reference yield:

: 179260-96-9
4-methoxy-3-(triisopropylsilyloxy)-benzaldehyde

: 1622094-35-2
C₁₇H₂₇IO₄Si

Guidance literature:: Multi-step reaction with 2 steps

1: silver nitrate; iodine / dichloromethane / 14 h / 20 °C / Inert atmosphere

2: copper dichloride; tert.-butylhydroperoxide / acetonitrile; water / 16 h / 20 - 50 °C

With tert.-butylhydroperoxide; iodine; silver nitrate; copper dichloride; In dichloromethane; water; acetonitrile;
DOI:10.1002/chem.201402323

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 1622094-35-2
C₁₇H₂₇IO₄Si

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

2: silver nitrate; iodine / dichloromethane / 14 h / 20 °C / Inert atmosphere

3: copper dichloride; tert.-butylhydroperoxide / acetonitrile; water / 16 h / 20 - 50 °C

With 1H-imidazole; tert.-butylhydroperoxide; iodine; silver nitrate; copper dichloride; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201402323