Technology Process of C18H14F2N2O6
There total 11 articles about C18H14F2N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetra(n-butyl)ammonium hydroxide; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
dichloromethane;
pH=Ca. 4;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 1.5 h / 0 - 20 °C
2: pyridine / 12 h / 0 - 20 °C
3: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; tetra(n-butyl)ammonium hydroxide / dichloromethane / pH Ca. 4
With
pyridine; N-iodo-succinimide; tetra(n-butyl)ammonium hydroxide; triethylamine tris(hydrogen fluoride); 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 1 h / 20 °C
2: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 1.5 h / 0 - 20 °C
3: pyridine / 12 h / 0 - 20 °C
4: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; tetra(n-butyl)ammonium hydroxide / dichloromethane / pH Ca. 4
With
pyridine; N-iodo-succinimide; tetra(n-butyl)ammonium hydroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; acetonitrile;