2-nitro-3,4,5,6-tetrabromoanisole

Base Information

Chemical Name:2-nitro-3,4,5,6-tetrabromoanisole
CAS No.:6161-58-6
Molecular Formula:C₇H₃Br₄NO₃
Molecular Weight:468.722
Hs Code.:

Synonyms:2-nitro-3,4,5,6-tetrabromoanisole

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Chemical Property of 2-nitro-3,4,5,6-tetrabromoanisole

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Technology Process of 2-nitro-3,4,5,6-tetrabromoanisole

There total 6 articles about 2-nitro-3,4,5,6-tetrabromoanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 6161-61-1
2,3,4,5-tetrabromoanisole

: 6161-58-6
2-nitro-3,4,5,6-tetrabromoanisole

Guidance literature:: With nitric acid; In acetic anhydride; at 35 - 40 ℃; for 1.3h;
DOI:10.1007/BF01151297

Reference yield:

: 15969-09-2
2,4-dibromo-6-nitrophenol

: 6161-58-6
2-nitro-3,4,5,6-tetrabromoanisole

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / ethanol / 20 °C

1.2: 1.25 h

2.1: hydrogenchloride; tin(ll) chloride / acetic acid / 6 h / 70 - 80 °C

3.1: hydrogenchloride; tin(ll) chloride / acetic acid / 6 h / 70 - 80 °C

3.2: 1.5 h / 50 °C

4.1: hydrogenchloride; tin(ll) chloride / acetic acid / 6 h / 70 - 80 °C

4.2: 1.5 h / 50 °C

5.1: nitric acid / acetic anhydride / 0.03 h

With hydrogenchloride; nitric acid; tin(ll) chloride; potassium hydroxide; In ethanol; acetic anhydride; acetic acid;
DOI:10.1134/S1070428012080064

Reference yield:

: 3,4,5,6-tetrabromo-2-methoxyaniline

: 6161-58-6
2-nitro-3,4,5,6-tetrabromoanisole

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; tin(ll) chloride / acetic acid / 6 h / 70 - 80 °C

1.2: 1.5 h / 50 °C

2.1: nitric acid / acetic anhydride / 0.03 h

With hydrogenchloride; nitric acid; tin(ll) chloride; In acetic anhydride; acetic acid;
DOI:10.1134/S1070428012080064