triethylammonium 1,2-di-O-benzyl-sn-glyceryl 2,3-O-isopropylidene-sn-glycerylphosphate

Base Information

• Chemical Name: triethylammonium 1,2-di-O-benzyl-sn-glyceryl 2,3-O-isopropylidene-sn-glycerylphosphate
• CAS No.: 1360874-31-2
• Molecular Formula: C₆H₁₅N*C₂₃H₃₁O₈P
• Molecular Weight: 567.66

Synonyms:triethylammonium 1,2-di-O-benzyl-sn-glyceryl 2,3-O-isopropylidene-sn-glycerylphosphate

Chemical Property of triethylammonium 1,2-di-O-benzyl-sn-glyceryl 2,3-O-isopropylidene-sn-glycerylphosphate

Chemical Property:

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Technology Process of triethylammonium 1,2-di-O-benzyl-sn-glyceryl 2,3-O-isopropylidene-sn-glycerylphosphate

There total 3 articles about triethylammonium 1,2-di-O-benzyl-sn-glyceryl 2,3-O-isopropylidene-sn-glycerylphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

triethylammonium 1,2-di-O-benzyl-sn-glyceryl hydrogenphosphonate (141263-13-0) + (S)-(+)-(2,2-dimethyl-[1,3]dioxolan-4-yl)methanol (22323-82-6,36543-79-0) → triethylammonium 1,2-di-O-benzyl-sn-glyceryl 2,3-O-isopropylidene-sn-glycerylphosphate (1360874-31-2)

Guidance literature:

triethylammonium 1,2-di-O-benzyl-sn-glyceryl hydrogenphosphonate; (S)-(+)-(2,2-dimethyl-[1,3]dioxolan-4-yl)methanol; With pyridine; pivaloyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 0.0333333h;

With pyridine; iodine; In tetrahydrofuran; water; at 20 ℃; for 0.5h;

DOI:10.1002/anie.201106470

Reference yield:

(R)-2,3-dibenzyloxy-1-propanol (58530-76-0) → triethylammonium 1,2-di-O-benzyl-sn-glyceryl 2,3-O-isopropylidene-sn-glycerylphosphate (1360874-31-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: pyridine; diphenyl phosphite / 1.17 h / 0 - 20 °C

1.2: 1 h / 20 °C

2.1: pyridine; pivaloyl chloride / tetrahydrofuran / 0.03 h / 0 - 20 °C

2.2: 0.5 h / 20 °C

With pyridine; diphenyl phosphite; pivaloyl chloride; In tetrahydrofuran;

DOI:10.1002/anie.201106470

Reference yield:

triethylamine (121-44-8) → triethylammonium 1,2-di-O-benzyl-sn-glyceryl 2,3-O-isopropylidene-sn-glycerylphosphate (1360874-31-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: pyridine; diphenyl phosphite / 1.17 h / 0 - 20 °C

1.2: 1 h / 20 °C

2.1: pyridine; pivaloyl chloride / tetrahydrofuran / 0.03 h / 0 - 20 °C

2.2: 0.5 h / 20 °C

With pyridine; diphenyl phosphite; pivaloyl chloride; In tetrahydrofuran;

DOI:10.1002/anie.201106470

upstream raw materials:

triethylammonium 1,2-di-O-benzyl-sn-glyceryl hydrogenphosphonate

(S)-(+)-(2,2-dimethyl-[1,3]dioxolan-4-yl)methanol

(R)-2,3-dibenzyloxy-1-propanol

triethylamine

Downstream raw materials:

triethylammonium 1,2-di-O-benzyl-sn-glyceryl 1-sn-glyceryl phosphate

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