4-amino-5,6-dimethyl-7-phenyl-7H-pyrrolo<2,3-d>pyrimidine-2-methylsulfone

Base Information

Chemical Name:4-amino-5,6-dimethyl-7-phenyl-7H-pyrrolo<2,3-d>pyrimidine-2-methylsulfone
CAS No.:111601-27-5
Molecular Formula:C₁₅H₁₆N₄O₂S
Molecular Weight:316.384
Hs Code.:

Synonyms:4-amino-5,6-dimethyl-7-phenyl-7H-pyrrolo<2,3-d>pyrimidine-2-methylsulfone

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Chemical Property of 4-amino-5,6-dimethyl-7-phenyl-7H-pyrrolo<2,3-d>pyrimidine-2-methylsulfone

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Technology Process of 4-amino-5,6-dimethyl-7-phenyl-7H-pyrrolo<2,3-d>pyrimidine-2-methylsulfone

There total 7 articles about 4-amino-5,6-dimethyl-7-phenyl-7H-pyrrolo<2,3-d>pyrimidine-2-methylsulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 111601-26-4
5,6-dimethyl-2-methylthio-7-phenyl-7H-pyrrolo<2,3-d>pyrimidine-4-amine

: 111601-27-5
4-amino-5,6-dimethyl-7-phenyl-7H-pyrrolo<2,3-d>pyrimidine-2-methylsulfone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In ethanol; for 12h; Ambient temperature;

Reference yield:

: 54329-29-2
2-Amino-3-cyano-4,5-dimethyl-1-phenylpyrrole

: 111601-27-5
4-amino-5,6-dimethyl-7-phenyl-7H-pyrrolo<2,3-d>pyrimidine-2-methylsulfone

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / pyridine / 2 h / Heating

2: 96 percent / methanol / 1 h / Heating

3: 57 percent / 5percent aq.KOH / 1 h / Ambient temperature

4: 100 percent / NH₃(l) / 3 h / 100 °C / steel vessel

5: 96 percent / m-chloroperoxybenzoic acid / ethanol / 12 h / Ambient temperature

With potassium hydroxide; ammonia; 3-chloro-benzenecarboperoxoic acid; In pyridine; methanol; ethanol;

Reference yield:

: 4-imino-5,6-dimethyl-7-phenyl-4,7-dihydropyrrolo<2,3-d><1,3>thiazine-2(1H)-thione

: 111601-27-5
4-amino-5,6-dimethyl-7-phenyl-7H-pyrrolo<2,3-d>pyrimidine-2-methylsulfone

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / methanol / 1 h / Heating

2: 57 percent / 5percent aq.KOH / 1 h / Ambient temperature

3: 100 percent / NH₃(l) / 3 h / 100 °C / steel vessel

4: 96 percent / m-chloroperoxybenzoic acid / ethanol / 12 h / Ambient temperature

With potassium hydroxide; ammonia; 3-chloro-benzenecarboperoxoic acid; In methanol; ethanol;