Bis(4-methoxy-2-nitrophenyl)diselenide

Base Information

• Chemical Name: Bis(4-methoxy-2-nitrophenyl)diselenide
• CAS No.: 35350-45-9
• Molecular Formula: C14H12 N2 O6 Se2
• Molecular Weight: 462.179
• Hs Code.: 2909309090
• DSSTox Substance ID: DTXSID30369930
• Wikidata: Q82157219
• Mol file: 35350-45-9.mol

Synonyms:Bis(4-methoxy-2-nitrophenyl)diselenide;35350-45-9;1,2-bis(4-methoxy-2-nitrophenyl)diselane;4-methoxy-1-[(4-methoxy-2-nitrophenyl)diselanyl]-2-nitrobenzene;DTXSID30369930;MFCD00775972;AKOS001021074;FT-0761213;BIS-(4-METHOXY-2-NITROPHENYL)DISELENIDE;Z56794904;F0400-0032;3-Chloro-6-(2-hydroxy-ethyl)-pyrazolo[1,5-a]-pyrimidine-2-carboxylicacid

Chemical Property of Bis(4-methoxy-2-nitrophenyl)diselenide

Chemical Property:

• Vapor Pressure: 8.8E-14mmHg at 25°C
• Melting Point: 173°C
• Boiling Point: 601.4°C at 760 mmHg
• Flash Point: 317.5°C
• PSA: 110.10000
• LogP: 1.84080
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 5
• Exact Mass: 463.90258
• Heavy Atom Count: 24
• Complexity: 404

Purity/Quality:

98%Min ^*data from raw suppliers

BIS(4-METHOXY-2-NITROPHENYL)DISELENIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC(=C(C=C1)[Se][Se]C2=C(C=C(C=C2)OC)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of Bis(4-methoxy-2-nitrophenyl)diselenide

There total 6 articles about Bis(4-methoxy-2-nitrophenyl)diselenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

2-chloro-5-methoxynitrobenzene (10298-80-3) → bis(4-methoxy-2-nitrophenyl) diselenide (35350-45-9)

Guidance literature:

With selenium; sodium thiosulfate; In dimethyl sulfoxide; at 60 ℃; for 24h;

Reference yield:

4-methoxy-2-nitro-phenyl selenocyanate (63816-14-8) → bis(4-methoxy-2-nitrophenyl) diselenide (35350-45-9)

Guidance literature:

With sodium hydroxide;

Reference yield:

bis-(4-methoxy-2-nitro-phenyl)-triselenide (859322-91-1) → bis(4-methoxy-2-nitrophenyl) diselenide (35350-45-9)

Guidance literature:

at 200 ℃;

upstream raw materials:

bis-(4-methoxy-2-nitro-phenyl)-triselenide

4-methoxy-2-nitro-phenyl selenocyanate

2-chloro-5-methoxynitrobenzene

4-methoxy-2-nitro-benzeneselenenyl bromide

Downstream raw materials:

(4-methoxy-2-nitro-phenyl)-thiocyanato-selane

4-methoxy-2-nitro-benzeneselenenic acid

bis(4-methoxy-2-aminophenyl) diselenide

4-methoxy-2-nitro-benzeneselenenyl bromide

Refernces