(1,2-bis(diphenylphosphino)ethane-P,P)(η2-2,2-dimethylpropylidynephosphine-P',C)-platinum(0)-P-pentacarbonyltungsten(0)

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Chemical Name:(1,2-bis(diphenylphosphino)ethane-P,P)(η2-2,2-dimethylpropylidynephosphine-P',C)-platinum(0)-P-pentacarbonyltungsten(0)
CAS No.:150694-66-9
Molecular Formula:C₃₆H₃₃O₅P₃PtW
Molecular Weight:1017.51
Hs Code.:

Synonyms:(1,2-bis(diphenylphosphino)ethane-P,P)(η2-2,2-dimethylpropylidynephosphine-P',C)-platinum(0)-P-pentacarbonyltungsten(0)

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Chemical Property of (1,2-bis(diphenylphosphino)ethane-P,P)(η2-2,2-dimethylpropylidynephosphine-P',C)-platinum(0)-P-pentacarbonyltungsten(0)

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Technology Process of (1,2-bis(diphenylphosphino)ethane-P,P)(η2-2,2-dimethylpropylidynephosphine-P',C)-platinum(0)-P-pentacarbonyltungsten(0)

There total 2 articles about (1,2-bis(diphenylphosphino)ethane-P,P)(η2-2,2-dimethylpropylidynephosphine-P',C)-platinum(0)-P-pentacarbonyltungsten(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.6%

: 14040-11-0
tungsten hexacarbonyl

: {(1,2-bis(diphenylphosphino)ethane-P,P)(2,2-dimethylpropylidynephosphine-P,C)}platinum⁽⁰⁾

: 150694-66-9
(1,2-bis(diphenylphosphino)ethane-P,P)(η2-2,2-dimethylpropylidynephosphine-P',C)-platinum(0)-P-pentacarbonyltungsten(0)

Guidance literature:: With tetrahydrofuran; In tetrahydrofuran; W(CO)6 reacted with THF to (W(CO)5THF), to the excess of the soln. added Pt-compound, mixture stirred for 2 h at room temp.; solvent removed, washed several times with petroleum ether (60-80°); elem. anal.;
DOI:10.1016/0022-328X(93)83113-A

Reference yield: 71.0%

: 12129-25-8
(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonyltungsten⁽⁰⁾

: {(1,2-bis(diphenylphosphino)ethane-P,P)(2,2-dimethylpropylidynephosphine-P,C)}platinum⁽⁰⁾

: 150694-66-9
(1,2-bis(diphenylphosphino)ethane-P,P)(η2-2,2-dimethylpropylidynephosphine-P',C)-platinum(0)-P-pentacarbonyltungsten(0)

Guidance literature:: In tetrahydrofuran; soln. of Pt-compound in THF treated with excess of W-complex, mixture stirred for 12 h at room temp.; solvent pumped to dryness, washed several times with petroleum ether (60-80°);
DOI:10.1016/0022-328X(93)83113-A