Technology Process of butyl 3-{2-[(2-pyridyl)thio]phenyl}acrylate
There total 5 articles about butyl 3-{2-[(2-pyridyl)thio]phenyl}acrylate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium chloride; zinc;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1002/chem.201003633
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / dimethyl sulfoxide / 18 h / 110 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere
3: dipotassium peroxodisulfate; palladium diacetate / 1,2-dichloro-ethane / 20 h / 110 °C / Inert atmosphere
4: ammonium chloride; zinc / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
With
dipotassium peroxodisulfate; palladium diacetate; potassium carbonate; ammonium chloride; 3-chloro-benzenecarboperoxoic acid; zinc;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1002/chem.201003633
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere
2: dipotassium peroxodisulfate; palladium diacetate / 1,2-dichloro-ethane / 20 h / 110 °C / Inert atmosphere
3: ammonium chloride; zinc / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
With
dipotassium peroxodisulfate; palladium diacetate; ammonium chloride; 3-chloro-benzenecarboperoxoic acid; zinc;
In
tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/chem.201003633
