(O₂NC₆H₄)CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))⁽¹⁺⁾*BF₄^(1-)=[O₂NC₆H₄CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))]BF₄

Base Information

• Chemical Name: (O₂NC₆H₄)CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))⁽¹⁺⁾*BF₄^(1-)=[O₂NC₆H₄CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))]BF₄
• CAS No.: 207301-29-9
• Molecular Formula: BF₄*C₁₉H₁₈FeN₅O₂
• Molecular Weight: 491.036

Synonyms:(O₂NC₆H₄)CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))⁽¹⁺⁾*BF₄^(1-)=[O₂NC₆H₄CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))]BF₄

Chemical Property of (O₂NC₆H₄)CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))⁽¹⁺⁾*BF₄^(1-)=[O₂NC₆H₄CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))]BF₄

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Technology Process of (O₂NC₆H₄)CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))⁽¹⁺⁾*BF₄^(1-)=[O₂NC₆H₄CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))]BF₄

There total 1 articles about (O₂NC₆H₄)CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))⁽¹⁺⁾*BF₄^(1-)=[O₂NC₆H₄CN₄H(CH(CH₃)(C₅H₄)Fe(C₅H₅))]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

tetrafluoroboric acid + 1-ferrocenylethanol (1277-49-2) + 5-(4-nitrophenyl)-1H-1,2,3,4-tetrazole (16687-60-8) → (O2NC6H4)CN4H(CH(CH3)(C5H4)Fe(C5H5))(1+)*BF4(1-)=[O2NC6H4CN4H(CH(CH3)(C5H4)Fe(C5H5))]BF4 (207301-29-9)

Guidance literature:

In dichloromethane; water; aq. soln. of HBF4 addn. to soln. of Fe-compd. and tetrazole in CH2Cl2 with vigorous stirring, reaction time 15 min; hexane-diethyl ether addn., ppt. filtration off, washing (cooled water),vacuum drying (over P2O5); elem. anal.;

Reference yield:

(O2NC6H4)CN4H(CH(CH3)(C5H4)Fe(C5H5))(1+)*BF4(1-)=[O2NC6H4CN4H(CH(CH3)(C5H4)Fe(C5H5))]BF4 (207301-29-9) → 1-ferrocenylethanol (1277-49-2) + 5-(4-nitrophenyl)-1H-1,2,3,4-tetrazole (16687-60-8)

Guidance literature:

With sodium hydroxide; In water; refluxing (5-10 min), cooling to 5 to 7°C; ppt. filtration off, washing (hot pentane), Fe-compd. obtaining from pentane extracts by drying, tetrazole remaining in the solid residue;

upstream raw materials:

1-ferrocenylethanol

5-(4-nitrophenyl)-1H-1,2,3,4-tetrazole

Downstream raw materials:

1-ferrocenylethanol

5-(4-nitrophenyl)-1H-1,2,3,4-tetrazole

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