N-(4-Chlorophenyl)-5,6-dimethylthieno[2,3-d]pyrimidin-4-amine

Base Information

Chemical Name:N-(4-Chlorophenyl)-5,6-dimethylthieno[2,3-d]pyrimidin-4-amine
CAS No.:309732-64-7
Molecular Formula:C₁₄H₁₂ClN₃S
Molecular Weight:289.788
Hs Code.:
Mol file:309732-64-7.mol

Synonyms:N-(4-Chlorophenyl)-5,6-dimethylthieno[2,3-d]pyrimidin-4-amine

Suppliers and Price of N-(4-Chlorophenyl)-5,6-dimethylthieno[2,3-d]pyrimidin-4-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

American Custom Chemicals Corporation
N-(4-CHLOROPHENYL)-5,6-DIMETHYLTHIENO[2,3-D]PYRIMIDIN-4-AMINE 95.00%
5MG
$ 500.38

Total 0 raw suppliers

Chemical Property of N-(4-Chlorophenyl)-5,6-dimethylthieno[2,3-d]pyrimidin-4-amine

Chemical Property:

Purity/Quality:: N-(4-CHLOROPHENYL)-5,6-DIMETHYLTHIENO[2,3-D]PYRIMIDIN-4-AMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of N-(4-Chlorophenyl)-5,6-dimethylthieno[2,3-d]pyrimidin-4-amine

There total 3 articles about N-(4-Chlorophenyl)-5,6-dimethylthieno[2,3-d]pyrimidin-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 106-47-8
4-chloro-aniline

: 108831-68-1
4-chloro-5,6-dimethyl-thieno[2,3-d]pyrimidine

: 309732-64-7
N-(4-Chlorophenyl)-5,6-dimethylthieno[2,3-d]pyrimidin-4-amine

Guidance literature:: In isopropyl alcohol; at 100 ℃; for 0.4h; Microwave irradiation;
DOI:10.1111/cbdd.13028

Reference yield:

: 4815-24-1
2-amino-4,5-dimethyl-3-thiophenecarboxylic acid ethyl ester

: 309732-64-7
N-(4-Chlorophenyl)-5,6-dimethylthieno[2,3-d]pyrimidin-4-amine

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / Cooling with ice; Microwave irradiation

2: isopropyl alcohol / 0.67 h / Microwave irradiation

With trichlorophosphate; In isopropyl alcohol; 1: |Vilsmeier-Haack Formylation;
DOI:10.1080/00397911.2011.607934

Reference yield:

: 18593-44-7
5,6-dimethylthieno<2,3-d>pyrimidin-4(3H)-one

: 309732-64-7
N-(4-Chlorophenyl)-5,6-dimethylthieno[2,3-d]pyrimidin-4-amine

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 100 °C / Microwave irradiation

2: isopropyl alcohol / 0.4 h / 100 °C / Microwave irradiation

With trichlorophosphate; In isopropyl alcohol;
DOI:10.1111/cbdd.13028