N-(3-azidopropyl)-3-(tert-butyldimethylsilyloxymethyl)-2-nitrobenzamide

Base Information

Chemical Name:N-(3-azidopropyl)-3-(tert-butyldimethylsilyloxymethyl)-2-nitrobenzamide
CAS No.:1259533-65-7
Molecular Formula:C₁₇H₂₇N₅O₄Si
Molecular Weight:393.518
Hs Code.:

Synonyms:N-(3-azidopropyl)-3-(tert-butyldimethylsilyloxymethyl)-2-nitrobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-azidopropyl)-3-(tert-butyldimethylsilyloxymethyl)-2-nitrobenzamide

Chemical Property:

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Technology Process of N-(3-azidopropyl)-3-(tert-butyldimethylsilyloxymethyl)-2-nitrobenzamide

There total 1 articles about N-(3-azidopropyl)-3-(tert-butyldimethylsilyloxymethyl)-2-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 88192-19-2
3-azidopropylamine

: 936943-03-2
3-(tert-butyldimethylsilyloxymethyl)-2-nitrobenzoic acid

: 1259533-65-7
N-(3-azidopropyl)-3-(tert-butyldimethylsilyloxymethyl)-2-nitrobenzamide

Guidance literature:: 3-(tert-butyldimethylsilyloxymethyl)-2-nitrobenzoic acid; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;

3-azidopropylamine; In dichloromethane; toluene; at 20 ℃; Inert atmosphere;
DOI:10.1021/ma1021506

Reference yield: 78.0%

: 1259533-65-7
N-(3-azidopropyl)-3-(tert-butyldimethylsilyloxymethyl)-2-nitrobenzamide

: 1259533-68-0
N-(3-azidopropyl)-3-(hydroxymethyl)-2-nitrobenzamide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/ma1021506

Reference yield:

: 1259533-65-7
N-(3-azidopropyl)-3-(tert-butyldimethylsilyloxymethyl)-2-nitrobenzamide

: 1259533-71-5
C₁₈H₁₆N₆O₈

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran

2: triethylamine / tetrahydrofuran / 0.25 h

With tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran;
DOI:10.1021/ma1021506