2'-[(S)-2-(4-Hydroxy-phenyl)-1-methoxycarbonyl-ethylcarbamoyl]-biphenyl-2-carboxylic acid

Base Information

Chemical Name:2'-[(S)-2-(4-Hydroxy-phenyl)-1-methoxycarbonyl-ethylcarbamoyl]-biphenyl-2-carboxylic acid
CAS No.:794589-63-2
Molecular Formula:C₂₄H₂₁NO₆
Molecular Weight:419.434
Hs Code.:

Synonyms:2'-[(S)-2-(4-Hydroxy-phenyl)-1-methoxycarbonyl-ethylcarbamoyl]-biphenyl-2-carboxylic acid

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Chemical Property of 2'-[(S)-2-(4-Hydroxy-phenyl)-1-methoxycarbonyl-ethylcarbamoyl]-biphenyl-2-carboxylic acid

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Technology Process of 2'-[(S)-2-(4-Hydroxy-phenyl)-1-methoxycarbonyl-ethylcarbamoyl]-biphenyl-2-carboxylic acid

There total 1 articles about 2'-[(S)-2-(4-Hydroxy-phenyl)-1-methoxycarbonyl-ethylcarbamoyl]-biphenyl-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 6050-13-1
biphenyl-2,2'-dicarboxylic acid anhydride

: 1080-06-4
L-Tyr-OMe

: 794589-63-2
2'-[(S)-2-(4-Hydroxy-phenyl)-1-methoxycarbonyl-ethylcarbamoyl]-biphenyl-2-carboxylic acid

Guidance literature:: With 2,4,6-trimethyl-pyridine; In N,N-dimethyl-formamide; at 20 ℃; for 15h;
DOI:10.1016/j.bmcl.2004.03.071

Reference yield: 94.0%

: 794589-63-2
2'-[(S)-2-(4-Hydroxy-phenyl)-1-methoxycarbonyl-ethylcarbamoyl]-biphenyl-2-carboxylic acid

: Phe-Cys-OMe trifluoroacetate

: (S)-2-[(S)-2-({2'-[(S)-2-(4-Hydroxy-phenyl)-1-methoxycarbonyl-ethylcarbamoyl]-biphenyl-2-carbonyl}-amino)-3-phenyl-propionylamino]-4-methylsulfanyl-butyric acid methyl ester

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; dmap; In N,N-dimethyl-formamide; at 20 ℃; for 32h;
DOI:10.1016/j.bmcl.2004.03.071

Reference yield:

: 794589-63-2
2'-[(S)-2-(4-Hydroxy-phenyl)-1-methoxycarbonyl-ethylcarbamoyl]-biphenyl-2-carboxylic acid

: (S)-2-{(S)-2-[2-((2S,3S,6S)-2-Allyloxy-6-aminomethyl-3,6-dihydro-2H-pyran-3-yl)-acetylamino]-3-phenyl-propionylamino}-4-methyl-pentanoic acid methylamide

: (S)-2-({2'-[((2S,5S,6S)-6-Allyloxy-5-{[(S)-1-((S)-3-methyl-1-methylcarbamoyl-butylcarbamoyl)-2-phenyl-ethylcarbamoyl]-methyl}-5,6-dihydro-2H-pyran-2-ylmethyl)-carbamoyl]-biphenyl-2-carbonyl}-amino)-3-(4-hydroxy-phenyl)-propionic acid methyl ester

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; dmap; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmcl.2004.03.071