Technology Process of C30H33NO7
There total 4 articles about C30H33NO7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Oxone; C13H20O9; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate;
In
Dimethoxymethane; water; acetonitrile;
at 0 ℃;
for 24h;
pH=6;
optical yield given as %de;
diastereoselective reaction;
aq. phosphate buffer;
DOI:10.1002/anie.201006528
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C
2.2: 2.5 h / 20 °C
3.1: Oxone; C13H20O9; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer
With
Oxone; sodium tetrahydroborate; C13H20O9; tetra(n-butyl)ammonium hydrogensulfate; sodium hydride; potassium carbonate;
In
tetrahydrofuran; methanol; Dimethoxymethane; water; acetonitrile; mineral oil;
3.1: Shi epoxidation;
DOI:10.1002/anie.201006528
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C
1.2: 2.5 h / 20 °C
2.1: Oxone; C13H20O9; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer
With
Oxone; C13H20O9; tetra(n-butyl)ammonium hydrogensulfate; sodium hydride; potassium carbonate;
In
tetrahydrofuran; Dimethoxymethane; water; acetonitrile; mineral oil;
2.1: Shi epoxidation;
DOI:10.1002/anie.201006528
