C₂₆H₃₃N₃O₅

Base Information

Chemical Name:C₂₆H₃₃N₃O₅
CAS No.:1444003-32-0
Molecular Formula:C₂₆H₃₃N₃O₅
Molecular Weight:467.565
Hs Code.:

C<sub>26</sub>H<sub>33</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₆H₃₃N₃O₅

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Chemical Property of C₂₆H₃₃N₃O₅

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Technology Process of C₂₆H₃₃N₃O₅

There total 3 articles about C₂₆H₃₃N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1444003-20-6
(S)-N-(2-acetylphenyl)-3-(3,4-dimethoxyphenyl)-2-(1H-pyrrol-1-yl)propanamide

: 33797-51-2
eschenmoser's salt

: 1444003-32-0
C₂₆H₃₃N₃O₅

Guidance literature:: (S)-N-(2-acetylphenyl)-3-(3,4-dimethoxyphenyl)-2-(1H-pyrrol-1-yl)propanamide; With water; In acetonitrile; at 0 ℃; UV-irradiation;

eschenmoser's salt; With trifluoroacetic acid; In acetonitrile;
DOI:10.1021/ja4042109

Reference yield:

: 32161-30-1
(S)-3,4-dimethoxyphenylalanine

: 1444003-32-0
C₂₆H₃₃N₃O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; sodium acetate / 1,2-dichloro-ethane / 0.08 h / 90 °C

1.2: 90 °C

2.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.08 h / 20 °C

3.1: water / acetonitrile / 0 °C / UV-irradiation

With 1-hydroxy-7-aza-benzotriazole; water; sodium acetate; acetic acid; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja4042109

Reference yield:

: 1444003-11-5
(S)-3-(3,4-dimethoxyphenyl)-2-(1H-pyrrol-1-yl)propanoic acid

: 1444003-32-0
C₂₆H₃₃N₃O₅

Guidance literature:: Multi-step reaction with 2 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.08 h / 20 °C

2: water / acetonitrile / 0 °C / UV-irradiation

With 1-hydroxy-7-aza-benzotriazole; water; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja4042109