C₁₆H₂₂N₂O

Base Information

Chemical Name:C₁₆H₂₂N₂O
CAS No.:1374312-52-3
Molecular Formula:C₁₆H₂₂N₂O
Molecular Weight:258.363
Hs Code.:

C<sub>16</sub>H<sub>22</sub>N<sub>2</sub>O

Synonyms:C₁₆H₂₂N₂O

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Chemical Property of C₁₆H₂₂N₂O

Chemical Property:

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Technology Process of C₁₆H₂₂N₂O

There total 6 articles about C₁₆H₂₂N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24123-89-5
(Z)-2-benzylidene-1-azabicyclo[2.2.2]octan-3-one

: 1374312-52-3
C₁₆H₂₂N₂O

: C₁₆H₂₂N₂O

Guidance literature:: Multi-step reaction with 6 steps

1.1: [N-[(1R,2R)-2-(amino-κN)-1,2-diphenylethyl]-4-methylbenzenesulfonamidato-κN]chloro[(1,2, 3,4,5,6-η)-1-methyl-4-(1-methylethyl)benzene]-ruthenium; water; sodium formate / isopropyl alcohol / 5 h / 67 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 1 h / 0 °C

3.1: tetrahydrofuran; toluene / 18 h / 107 °C

4.1: water; sodium hydroxide / ethanol / 25 °C / Large scale reaction

5.1: ethanol; water / 22 °C / Large scale reaction

5.2: Large scale reaction

6.1: palladium on activated charcoal; L-Tartaric acid; hydrogen / dichloromethane / 22 h / 35 °C / 5171.62 Torr

With [N-[(1R,2R)-2-(amino-κN)-1,2-diphenylethyl]-4-methylbenzenesulfonamidato-κN]chloro[(1,2, 3,4,5,6-η)-1-methyl-4-(1-methylethyl)benzene]-ruthenium; L-Tartaric acid; palladium on activated charcoal; water; hydrogen; sodium formate; sodium hexamethyldisilazane; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; isopropyl alcohol; toluene; 3.1: Overman rearrangement;
DOI:10.1021/op200378r

Reference yield:

: 1359842-43-5
(S)-N-[(1-azabicyclo[2.2.2]oct-2-en-2-yl)phenylmethyl]-acetamide

: 1374312-52-3
C₁₆H₂₂N₂O

: C₁₆H₂₂N₂O

Guidance literature:: With L-Tartaric acid; palladium on activated charcoal; hydrogen; In dichloromethane; at 35 ℃; for 22h; under 5171.62 Torr; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/op200378r

Reference yield:

: C₁₆H₁₇Cl₃N₂O

: 1374312-52-3
C₁₆H₂₂N₂O

: C₁₆H₂₂N₂O

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran; toluene / 18 h / 107 °C

2.1: water; sodium hydroxide / ethanol / 25 °C / Large scale reaction

3.1: ethanol; water / 22 °C / Large scale reaction

3.2: Large scale reaction

4.1: palladium on activated charcoal; L-Tartaric acid; hydrogen / dichloromethane / 22 h / 35 °C / 5171.62 Torr

With L-Tartaric acid; palladium on activated charcoal; water; hydrogen; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; 1.1: Overman rearrangement;
DOI:10.1021/op200378r