(E)-2-(4-chloro-2-fluoro-6-hydroxyphenyl)-2-phenylethenylphosphonic acid

Base Information

Chemical Name:(E)-2-(4-chloro-2-fluoro-6-hydroxyphenyl)-2-phenylethenylphosphonic acid
CAS No.:860279-17-0
Molecular Formula:C₁₄H₁₁ClFO₄P
Molecular Weight:328.664
Hs Code.:

Synonyms:(E)-2-(4-chloro-2-fluoro-6-hydroxyphenyl)-2-phenylethenylphosphonic acid

Suppliers and Price of (E)-2-(4-chloro-2-fluoro-6-hydroxyphenyl)-2-phenylethenylphosphonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-2-(4-chloro-2-fluoro-6-hydroxyphenyl)-2-phenylethenylphosphonic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-2-(4-chloro-2-fluoro-6-hydroxyphenyl)-2-phenylethenylphosphonic acid

There total 4 articles about (E)-2-(4-chloro-2-fluoro-6-hydroxyphenyl)-2-phenylethenylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 363-52-0
3-fluorocatechol

: 860279-17-0
(E)-2-(4-chloro-2-fluoro-6-hydroxyphenyl)-2-phenylethenylphosphonic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 55 percent / PCl₃ / 1 h / 80 °C

2: 100 percent / Cl₂ / CH₂Cl₂ / 12 Torr

3: 93 percent / CH₂Cl₂ / 3 h / 10 °C

4: 44 percent / water / diethyl ether / 24 h

5: 1.6 g / water / acetone / Heating

With water; chlorine; phosphorus trichloride; In diethyl ether; dichloromethane; acetone;
DOI:10.1007/s11178-005-0102-5

Reference yield:

: 860278-92-8
2-chloro-4-fluoro-1,3,2-benzodioxaphosphole

: 860279-17-0
(E)-2-(4-chloro-2-fluoro-6-hydroxyphenyl)-2-phenylethenylphosphonic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / Cl₂ / CH₂Cl₂ / 12 Torr

2: 93 percent / CH₂Cl₂ / 3 h / 10 °C

3: 44 percent / water / diethyl ether / 24 h

4: 1.6 g / water / acetone / Heating

With water; chlorine; In diethyl ether; dichloromethane; acetone;
DOI:10.1007/s11178-005-0102-5

Reference yield:

: 860278-87-1
2,2,2-trichloro-4-fluoro-1,3,2λ⁵-benzodioxaphosphole

: 860279-17-0
(E)-2-(4-chloro-2-fluoro-6-hydroxyphenyl)-2-phenylethenylphosphonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / CH₂Cl₂ / 3 h / 10 °C

2: 44 percent / water / diethyl ether / 24 h

3: 1.6 g / water / acetone / Heating

With water; In diethyl ether; dichloromethane; acetone;
DOI:10.1007/s11178-005-0102-5