toluene-4-sulfonic acid 2-(2-(4-(1-tert-butyl-5-chloro-6-oxo-1,6-dihydro-pyridazin-4-yloxymethyl)benzyloxy)ethoxy)ethyl ester

Base Information

• Chemical Name: toluene-4-sulfonic acid 2-(2-(4-(1-tert-butyl-5-chloro-6-oxo-1,6-dihydro-pyridazin-4-yloxymethyl)benzyloxy)ethoxy)ethyl ester
• CAS No.: 1194054-70-0
• Molecular Formula: C₂₆H₃₁ClN₂O₇S
• Molecular Weight: 551.06

Synonyms:toluene-4-sulfonic acid 2-(2-(4-(1-tert-butyl-5-chloro-6-oxo-1,6-dihydro-pyridazin-4-yloxymethyl)benzyloxy)ethoxy)ethyl ester

Chemical Property of toluene-4-sulfonic acid 2-(2-(4-(1-tert-butyl-5-chloro-6-oxo-1,6-dihydro-pyridazin-4-yloxymethyl)benzyloxy)ethoxy)ethyl ester

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Technology Process of toluene-4-sulfonic acid 2-(2-(4-(1-tert-butyl-5-chloro-6-oxo-1,6-dihydro-pyridazin-4-yloxymethyl)benzyloxy)ethoxy)ethyl ester

There total 2 articles about toluene-4-sulfonic acid 2-(2-(4-(1-tert-butyl-5-chloro-6-oxo-1,6-dihydro-pyridazin-4-yloxymethyl)benzyloxy)ethoxy)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

2-(tert-butyl)-4-chloro-5-((4-(2-(2-hydroxyethoxyl)ethoxy)benzyl)oxy)pyridazin-3(2H)-one (1194054-65-3) + p-toluenesulfonyl chloride (98-59-9) → toluene-4-sulfonic acid 2-(2-(4-(1-tert-butyl-5-chloro-6-oxo-1,6-dihydro-pyridazin-4-yloxymethyl)benzyloxy)ethoxy)ethyl ester (1194054-70-0)

Guidance literature:

With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 2h;

DOI:10.1016/j.bmc.2009.12.022

Reference yield: 19.0%

→ toluene-4-sulfonic acid 2-(2-(4-(1-tert-butyl-5-chloro-6-oxo-1,6-dihydro-pyridazin-4-yloxymethyl)benzyloxy)ethoxy)ethyl ester (1194054-70-0)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 55 ℃;

Reference yield: 80.0%

toluene-4-sulfonic acid 2-(2-(4-(1-tert-butyl-5-chloro-6-oxo-1,6-dihydro-pyridazin-4-yloxymethyl)benzyloxy)ethoxy)ethyl ester (1194054-70-0) → 2-(tert-butyl)-4-chloro-5-((4-(2-(2-fluoroethoxyl)ethoxy)benzyl)oxy)pyridazin-3(2H)-one (1194054-54-0)

Guidance literature:

With tetrabutyl ammonium fluoride; In acetonitrile; at 90 ℃; for 0.666667h;

DOI:10.1016/j.bmc.2009.12.022

upstream raw materials:

2-(tert-butyl)-4-chloro-5-((4-(2-(2-hydroxyethoxyl)ethoxy)benzyl)oxy)pyridazin-3(2H)-one

p-toluenesulfonyl chloride

Downstream raw materials:

2-(tert-butyl)-4-chloro-5-((4-(2-(2-fluoroethoxyl)ethoxy)benzyl)oxy)pyridazin-3(2H)-one

2-tert-butyl-5-{4-[2-(2-[⁽¹⁸⁾F]fluoroethoxy)ethoxy]benzyloxy}-4-chloro-2H-pyridazin-3-one

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