3-butyl-2-ethoxy-5,5-dimethyl-4-phenyl-2,5-dihydro-[1,2]oxaphosphole 2-oxide

Base Information

Chemical Name:3-butyl-2-ethoxy-5,5-dimethyl-4-phenyl-2,5-dihydro-[1,2]oxaphosphole 2-oxide
CAS No.:1103694-17-2
Molecular Formula:C₁₇H₂₅O₃P
Molecular Weight:308.357
Hs Code.:

Synonyms:3-butyl-2-ethoxy-5,5-dimethyl-4-phenyl-2,5-dihydro-[1,2]oxaphosphole 2-oxide

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Chemical Property of 3-butyl-2-ethoxy-5,5-dimethyl-4-phenyl-2,5-dihydro-[1,2]oxaphosphole 2-oxide

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Technology Process of 3-butyl-2-ethoxy-5,5-dimethyl-4-phenyl-2,5-dihydro-[1,2]oxaphosphole 2-oxide

There total 5 articles about 3-butyl-2-ethoxy-5,5-dimethyl-4-phenyl-2,5-dihydro-[1,2]oxaphosphole 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1103693-76-0
4-bromo-3-butyl-5,5-dimethyl-2-ethoxy-2,5-dihydro-[1,2]oxaphosphole 2-oxide

: 98-80-6
phenylboronic acid

: 1103694-17-2
3-butyl-2-ethoxy-5,5-dimethyl-4-phenyl-2,5-dihydro-[1,2]oxaphosphole 2-oxide

Guidance literature:: With potassium phosphate tribasic trihydrate; PdCl₂(SPhos)2; In toluene; for 1h; Reflux;
DOI:10.1021/jo802051r

Reference yield: 89.0%

: 937261-55-7
3-butyl-4-chloro-2-ethoxy-2,5-dihydro-5,5-dimethyl-1,2-oxaphosphole 2-oxide

: 98-80-6
phenylboronic acid

: 1103694-17-2
3-butyl-2-ethoxy-5,5-dimethyl-4-phenyl-2,5-dihydro-[1,2]oxaphosphole 2-oxide

Guidance literature:: With potassium phosphate tribasic trihydrate; PdCl₂(SPhos)2; In toluene; for 10h; Reflux;
DOI:10.1021/jo802051r

Reference yield: 9.0%

: 1103693-76-0
4-bromo-3-butyl-5,5-dimethyl-2-ethoxy-2,5-dihydro-[1,2]oxaphosphole 2-oxide

: 98-80-6
phenylboronic acid

: 3-butyl-2-ethoxy-5,5-dimethyl-5H-[1,2]oxaphosphole 2-oxide

: 1103694-17-2
3-butyl-2-ethoxy-5,5-dimethyl-4-phenyl-2,5-dihydro-[1,2]oxaphosphole 2-oxide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; for 22h; Reflux;
DOI:10.1021/jo802051r