O-(N',N'-dimethylcarbamoyl)-N-(tert-butoxycarbonyl)-2-chloro-4-aminophenol

Base Information

Chemical Name:O-(N',N'-dimethylcarbamoyl)-N-(tert-butoxycarbonyl)-2-chloro-4-aminophenol
CAS No.:1384312-89-3
Molecular Formula:C₁₄H₁₉ClN₂O₄
Molecular Weight:314.769
Hs Code.:

Synonyms:O-(N',N'-dimethylcarbamoyl)-N-(tert-butoxycarbonyl)-2-chloro-4-aminophenol

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Chemical Property of O-(N',N'-dimethylcarbamoyl)-N-(tert-butoxycarbonyl)-2-chloro-4-aminophenol

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Technology Process of O-(N',N'-dimethylcarbamoyl)-N-(tert-butoxycarbonyl)-2-chloro-4-aminophenol

There total 3 articles about O-(N',N'-dimethylcarbamoyl)-N-(tert-butoxycarbonyl)-2-chloro-4-aminophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 911297-03-5
N-(3-chloro-4-hydroxyphenyl)carbamic acid tert-butyl ester

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 1384312-89-3
O-(N',N'-dimethylcarbamoyl)-N-(tert-butoxycarbonyl)-2-chloro-4-aminophenol

Guidance literature:: With pyridine; at 70 ℃; for 25h; Inert atmosphere;
DOI:10.1021/ja303443m

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1384312-89-3
O-(N',N'-dimethylcarbamoyl)-N-(tert-butoxycarbonyl)-2-chloro-4-aminophenol

Guidance literature:: Multi-step reaction with 2 steps

1: water / 22 h / 20 °C

2: pyridine / 25 h / 70 °C / Inert atmosphere

With pyridine; In water;
DOI:10.1021/ja303443m

Reference yield:

: 3964-52-1
2-chloro 4-aminophenol

: 1384312-89-3
O-(N',N'-dimethylcarbamoyl)-N-(tert-butoxycarbonyl)-2-chloro-4-aminophenol

Guidance literature:: Multi-step reaction with 2 steps

1: water / 22 h / 20 °C

2: pyridine / 25 h / 70 °C / Inert atmosphere

With pyridine; In water;
DOI:10.1021/ja303443m