Ethanone, 1-[(1R,2R)-1-hydroxy-2-methyl-3-cyclohexen-1-yl]-, rel- (9CI)

Base Information

Chemical Name:Ethanone, 1-[(1R,2R)-1-hydroxy-2-methyl-3-cyclohexen-1-yl]-, rel- (9CI)
CAS No.:258266-09-0
Molecular Formula:C₉H₁₄O₂
Molecular Weight:154.209
Hs Code.:
Mol file:258266-09-0.mol

Synonyms:Ethanone, 1-[(1R,2R)-1-hydroxy-2-methyl-3-cyclohexen-1-yl]-, rel- (9CI)

Suppliers and Price of Ethanone, 1-[(1R,2R)-1-hydroxy-2-methyl-3-cyclohexen-1-yl]-, rel- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Ethanone, 1-[(1R,2R)-1-hydroxy-2-methyl-3-cyclohexen-1-yl]-, rel- (9CI)

Chemical Property:

PSA：37.30000
LogP:1.29260

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ethanone, 1-[(1R,2R)-1-hydroxy-2-methyl-3-cyclohexen-1-yl]-, rel- (9CI)

There total 4 articles about Ethanone, 1-[(1R,2R)-1-hydroxy-2-methyl-3-cyclohexen-1-yl]-, rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: (1R*,2R*)-1-acetyl-2-methyl-3-cyclohexen-1-yl p-nitrobenzoate

: 258266-09-0
(1R*,2R*)-1-acetyl-2-methyl-3-cyclohexen-1-ol

Guidance literature:: With potassium carbonate; In methanol; dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/S0040-4020(99)00928-X

Reference yield:

: 195200-19-2
2,4-Dinitro-benzoic acid 1-acetyl-2-methyl-cyclohex-3-enyl ester

: 258266-09-0
1-(1-Hydroxy-2-methyl-cyclohex-3-enyl)-ethanone

Guidance literature:: With potassium cyanide; In methanol; Ambient temperature;
DOI:10.1055/s-1997-5775

Reference yield:

: 504-60-9,17410-45-6,25212-15-1,64940-84-7
penta-1,3-diene

: 258266-09-0
(1R*,2R*)-1-acetyl-2-methyl-3-cyclohexen-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / AlCl₃ / CH₂Cl₂ / 8 h / 20 °C

2: 70 percent / K₂CO₃ / CH₂Cl₂; methanol / 2 h / 20 °C

With aluminium trichloride; potassium carbonate; In methanol; dichloromethane; 1: Cycloaddition / 2: Hydrolysis;
DOI:10.1016/S0040-4020(99)00928-X