2',3'-O-<<methyl>ethoxymethylidene>-N⁶-(4-aminobutyl)adenosine

Base Information

• Chemical Name: 2',3'-O-<<methyl>ethoxymethylidene>-N⁶-(4-aminobutyl)adenosine
• CAS No.: 73644-55-0
• Molecular Formula: C₂₆H₃₅N₇O₇
• Molecular Weight: 557.607

Synonyms:2',3'-O-<<methyl>ethoxymethylidene>-N⁶-(4-aminobutyl)adenosine

Chemical Property of 2',3'-O-<<methyl>ethoxymethylidene>-N⁶-(4-aminobutyl)adenosine

Chemical Property:

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Technology Process of 2',3'-O-<<methyl>ethoxymethylidene>-N⁶-(4-aminobutyl)adenosine

There total 1 articles about 2',3'-O-<<methyl>ethoxymethylidene>-N⁶-(4-aminobutyl)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

N6-(aminobutyl)adenosine (60687-66-3) + ethyl N-benzyloxycarbonylamino-orthoacetate (13347-35-8) → 2',3'-O-<<methyl>ethoxymethylidene>-N6-(4-aminobutyl)adenosine (73644-55-0)

Guidance literature:

With trifluoroacetic acid; In N,N-dimethyl-formamide; for 21h; Ambient temperature;

DOI:10.1021/jm00181a015

Reference yield: 40.0%

6-chloro-9-<2,3-O-(methoxyethylidene)-β-D-ribofuranosyl>purine (73644-53-8) + 2',3'-O-<<methyl>ethoxymethylidene>-N6-(4-aminobutyl)adenosine (73644-55-0) → 2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N6-yl)butane (73652-50-3)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; for 18h; Ambient temperature;

DOI:10.1021/jm00181a015

upstream raw materials:

N⁶-(aminobutyl)adenosine

ethyl N-benzyloxycarbonylamino-orthoacetate

Downstream raw materials:

2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N⁶-yl)butane

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