1-benzyl-3-(3-((3-(4-methoxyphenyl)prop-2-yn-1-yl)oxy)prop-1-yn-1-yl)-1H-indole

Base Information

Chemical Name:1-benzyl-3-(3-((3-(4-methoxyphenyl)prop-2-yn-1-yl)oxy)prop-1-yn-1-yl)-1H-indole
CAS No.:1599470-54-8
Molecular Formula:C₂₈H₂₃NO₂
Molecular Weight:405.496
Hs Code.:

Synonyms:1-benzyl-3-(3-((3-(4-methoxyphenyl)prop-2-yn-1-yl)oxy)prop-1-yn-1-yl)-1H-indole

Suppliers and Price of 1-benzyl-3-(3-((3-(4-methoxyphenyl)prop-2-yn-1-yl)oxy)prop-1-yn-1-yl)-1H-indole

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Chemical Property of 1-benzyl-3-(3-((3-(4-methoxyphenyl)prop-2-yn-1-yl)oxy)prop-1-yn-1-yl)-1H-indole

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Technology Process of 1-benzyl-3-(3-((3-(4-methoxyphenyl)prop-2-yn-1-yl)oxy)prop-1-yn-1-yl)-1H-indole

There total 6 articles about 1-benzyl-3-(3-((3-(4-methoxyphenyl)prop-2-yn-1-yl)oxy)prop-1-yn-1-yl)-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 887000-28-4
1-benzyl-3-iodo-1H-indole

: 1599470-54-8
1-benzyl-3-(3-((3-(4-methoxyphenyl)prop-2-yn-1-yl)oxy)prop-1-yn-1-yl)-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 3 h / 30 °C

2: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium hydride; triethylamine; In tetrahydrofuran; mineral oil; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/jo402749d

Reference yield:

: 696-62-8
para-iodoanisole

: 1599470-54-8
1-benzyl-3-(3-((3-(4-methoxyphenyl)prop-2-yn-1-yl)oxy)prop-1-yn-1-yl)-1H-indole

Guidance literature:: Multi-step reaction with 4 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 3 h / 30 °C

2: triethylamine / dichloromethane / 0 °C

3: lithium bromide / tetrahydrofuran

4: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium hydride; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; mineral oil; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/jo402749d

Reference yield:

: 924906-80-9
Methanesulfonic acid 3-(4-methoxy-phenyl)-prop-2-ynyl ester

: 1599470-54-8
1-benzyl-3-(3-((3-(4-methoxyphenyl)prop-2-yn-1-yl)oxy)prop-1-yn-1-yl)-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1: lithium bromide / tetrahydrofuran

2: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C

With sodium hydride; lithium bromide; In tetrahydrofuran; mineral oil;
DOI:10.1021/jo402749d