3-cyclohexyl-5,6,10,11-tetrahydro-8-methylbenzo[g]pyrazino[1,2-a]indole

Base Information

Chemical Name:3-cyclohexyl-5,6,10,11-tetrahydro-8-methylbenzo[g]pyrazino[1,2-a]indole
CAS No.:147031-26-3
Molecular Formula:C₂₂H₂₆N₂
Molecular Weight:318.462
Hs Code.:

Synonyms:3-cyclohexyl-5,6,10,11-tetrahydro-8-methylbenzo[g]pyrazino[1,2-a]indole

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Chemical Property of 3-cyclohexyl-5,6,10,11-tetrahydro-8-methylbenzo[g]pyrazino[1,2-a]indole

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Technology Process of 3-cyclohexyl-5,6,10,11-tetrahydro-8-methylbenzo[g]pyrazino[1,2-a]indole

There total 9 articles about 3-cyclohexyl-5,6,10,11-tetrahydro-8-methylbenzo[g]pyrazino[1,2-a]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 147581-70-2
2-(6-methoxy-1-oxo-1,2,3,4-tetrahydronaphthalen-2-yl)acetaldehyde

: 147031-26-3
3-cyclohexyl-5,6,10,11-tetrahydro-8-methylbenzo[g]pyrazino[1,2-a]indole

Guidance literature:: Multi-step reaction with 8 steps

1: molecular sieves 4 Angstroem / CH₂Cl₂

2: BBr₃ / CH₂Cl₂ / -25 °C

3: aq. NaHCO₃ / dioxane

4: POCl₃

5: n-PrNH₂ / CH₂Cl₂

6: NaH, DMA

7: (Ph₃P)2PdCl₂ / dimethylformamide / 120 °C

8: H₂, AcOH / 10percent Pd/C

With propylamine; bis-triphenylphosphine-palladium(II) chloride; 4 A molecular sieve; hydrogen; boron tribromide; 2,4-dichlorophenoxyacetic acid dimethylamine; sodium hydride; sodium hydrogencarbonate; acetic acid; trichlorophosphate; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 147031-07-0
2-((E)-But-2-enyl)-6-methoxy-3,4-dihydro-2H-naphthalen-1-one

: 147031-26-3
3-cyclohexyl-5,6,10,11-tetrahydro-8-methylbenzo[g]pyrazino[1,2-a]indole

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) O₃, 2.) Me₂S, 3.) aq. oxalic acid, silica gel

2: molecular sieves 4 Angstroem / CH₂Cl₂

3: BBr₃ / CH₂Cl₂ / -25 °C

4: aq. NaHCO₃ / dioxane

5: POCl₃

6: n-PrNH₂ / CH₂Cl₂

7: NaH, DMA

8: (Ph₃P)2PdCl₂ / dimethylformamide / 120 °C

9: H₂, AcOH / 10percent Pd/C

With propylamine; bis-triphenylphosphine-palladium(II) chloride; dimethylsulfide; 4 A molecular sieve; hydrogen; oxalic acid; silica gel; boron tribromide; 2,4-dichlorophenoxyacetic acid dimethylamine; sodium hydride; sodium hydrogencarbonate; ozone; acetic acid; trichlorophosphate; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 147031-24-1
5,6,10,11-tetrahydro-8-methyl-benzo[g]pyrazino[1,2-a]indol-3-ol

: 147031-26-3
3-cyclohexyl-5,6,10,11-tetrahydro-8-methylbenzo[g]pyrazino[1,2-a]indole

Guidance literature:: Multi-step reaction with 3 steps

1: NaH, DMA

2: (Ph₃P)2PdCl₂ / dimethylformamide / 120 °C

3: H₂, AcOH / 10percent Pd/C

With bis-triphenylphosphine-palladium(II) chloride; hydrogen; 2,4-dichlorophenoxyacetic acid dimethylamine; sodium hydride; acetic acid; palladium on activated charcoal; In N,N-dimethyl-formamide;