C₈H₅NS₂

Base Information

Chemical Name:C₈H₅NS₂
CAS No.:1423707-55-4
Molecular Formula:C₈H₅NS₂
Molecular Weight:179.266
Hs Code.:

C<sub>8</sub>H<sub>5</sub>NS<sub>2</sub>

Synonyms:C₈H₅NS₂

Suppliers and Price of C₈H₅NS₂

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Chemical Property of C₈H₅NS₂

Chemical Property:

Purity/Quality:

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Technology Process of C₈H₅NS₂

There total 1 articles about C₈H₅NS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930-96-1
3-bromo-2-thiophenecarboxaldehyde

: 1423707-55-4
C₈H₅NS₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 70 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

3.1: triphenylphosphine / dichloromethane / 0 - 20 °C / Inert atmosphere

3.2: 16 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1423707-55-4
C₈H₅NS₂

: 1620074-61-4
C₂₆H₂₃N₃O₄S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C / Inert atmosphere

1.2: 5 h / 0 - 20 °C / Inert atmosphere

2.1: lithium hydroxide / water / 16 h / Reflux

2.2: pH Ca_. 2

3.1: potassium carbonate / acetonitrile / 16 h / Reflux

4.1: N-iodo-succinimide; 2,6-dimethylpyridine / 20 °C

5.1: copper(l) iodide; triethylamine; phenylacetylene / N,N-dimethyl-formamide / 0.03 h

5.2: 2 h

With 2,6-dimethylpyridine; N-iodo-succinimide; copper(l) iodide; sodium hydride; potassium carbonate; triethylamine; phenylacetylene; lithium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 1423707-55-4
C₈H₅NS₂

: 1620070-13-4
C₃₁H₃₂N₄O₅S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C / Inert atmosphere

1.2: 5 h / 0 - 20 °C / Inert atmosphere

2.1: lithium hydroxide / water / 16 h / Reflux

2.2: pH Ca_. 2

3.1: potassium carbonate / acetonitrile / 16 h / Reflux

4.1: N-iodo-succinimide; 2,6-dimethylpyridine / 20 °C

5.1: lithium hydroxide monohydrate / tetrahydrofuran; water

6.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0.5 h

6.2: 3 h / 25 °C

7.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; dmap; bis-triphenylphosphine-palladium(II) chloride; N-iodo-succinimide; copper(l) iodide; lithium hydroxide monohydrate; sodium hydride; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;