1-(4-methoxybenzyl)-3-(4-methoxyphenyl)-5-octylpyrimidine-2,4,6(1H,3H,5H)-trione

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Chemical Name:1-(4-methoxybenzyl)-3-(4-methoxyphenyl)-5-octylpyrimidine-2,4,6(1H,3H,5H)-trione
CAS No.:933056-36-1
Molecular Formula:C₂₇H₃₄N₂O₅
Molecular Weight:466.577
Hs Code.:

Synonyms:1-(4-methoxybenzyl)-3-(4-methoxyphenyl)-5-octylpyrimidine-2,4,6(1H,3H,5H)-trione

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Chemical Property of 1-(4-methoxybenzyl)-3-(4-methoxyphenyl)-5-octylpyrimidine-2,4,6(1H,3H,5H)-trione

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Technology Process of 1-(4-methoxybenzyl)-3-(4-methoxyphenyl)-5-octylpyrimidine-2,4,6(1H,3H,5H)-trione

There total 4 articles about 1-(4-methoxybenzyl)-3-(4-methoxyphenyl)-5-octylpyrimidine-2,4,6(1H,3H,5H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 933056-60-1
N-(4-methoxyphenyl)-N'-(4-methoxybenzyl)carbodiimide

: 164533-78-2
2-octyl-malonic acid monoethyl ester

: 933056-36-1
1-(4-methoxybenzyl)-3-(4-methoxyphenyl)-5-octylpyrimidine-2,4,6(1H,3H,5H)-trione

Guidance literature:: N-(4-methoxyphenyl)-N'-(4-methoxybenzyl)carbodiimide; 2-octyl-malonic acid monoethyl ester; In 1,4-dioxane; at 20 ℃;

With sodium hydroxide; In 1,4-dioxane; at 20 ℃; for 1h;
DOI:10.1021/ol063074+

Reference yield:

: 2-octyl-malonic acid benzyl ester ethyl ester

: 933056-36-1
1-(4-methoxybenzyl)-3-(4-methoxyphenyl)-5-octylpyrimidine-2,4,6(1H,3H,5H)-trione

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / Pd(OH)2/C

2.1: dioxane / 20 °C

2.2: 83 percent / aq. NaOH / dioxane / 1 h / 20 °C

With hydrogen; palladium dihydroxide; In 1,4-dioxane;
DOI:10.1021/ol063074+

Reference yield:

: 111-83-1
1-bromo-octane

: 933056-36-1
1-(4-methoxybenzyl)-3-(4-methoxyphenyl)-5-octylpyrimidine-2,4,6(1H,3H,5H)-trione

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 0 - 20 °C

2.1: H₂ / Pd(OH)2/C

3.1: dioxane / 20 °C

3.2: 83 percent / aq. NaOH / dioxane / 1 h / 20 °C

With hydrogen; sodium hydride; palladium dihydroxide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/ol063074+