C₂₁H₃₃NO₄Si

Base Information

Chemical Name:C₂₁H₃₃NO₄Si
CAS No.:951776-48-0
Molecular Formula:C₂₁H₃₃NO₄Si
Molecular Weight:391.583
Hs Code.:

C<sub>21</sub>H<sub>33</sub>NO<sub>4</sub>Si

Synonyms:C₂₁H₃₃NO₄Si

Suppliers and Price of C₂₁H₃₃NO₄Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₁H₃₃NO₄Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₁H₃₃NO₄Si

There total 10 articles about C₂₁H₃₃NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 951776-47-9
C₂₁H₃₃NO₄Si

: 951776-48-0
C₂₁H₃₃NO₄Si

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; tungsten hexacarbonyl; In tetrahydrofuran; for 5h; Heating; UV-irradiation;
DOI:10.1021/ol7014219

Reference yield:

: C₂₆H₃₃NO₆Si

: 951776-48-0
C₂₁H₃₃NO₄Si

Guidance literature:: Multi-step reaction with 8 steps

1: 97 percent / MEli / diethyl ether; tetrahydrofuran / 0.5 h / -78 °C

2: 98 percent / imidazole; DMAP / CH₂Cl₂ / 1 h / 20 °C

3: 96 percent / tetrahydrofuran; diethyl ether / 2 h / -78 °C

4: 91 percent / K₂CO₃ / methanol / 1.5 h / 20 °C

5: 83 percent / CAN / acetonitrile; H₂O / 0.33 h / 20 °C

6: 98 percent / K₂CO₃ / acetone; H₂O / 2 h / 20 °C

7: 86 percent / NaBH₄; CeCl₃*7H₂O / CH₂Cl₂; methanol / -78 - 20 °C

8: 79 percent / DABCO / W(CO)6 / tetrahydrofuran / 5 h / Heating; UV-irradiation

With 1,4-diaza-bicyclo[2.2.2]octane; 1H-imidazole; dmap; sodium tetrahydroborate; cerium(III) chloride; ammonium cerium(IV) nitrate; methyllithium; potassium carbonate; tungsten hexacarbonyl; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; acetonitrile;
DOI:10.1021/ol7014219

Reference yield:

: 951776-74-2
C₂₂H₃₅NO₃Si₂

: 951776-48-0
C₂₁H₃₃NO₄Si

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / tetrahydrofuran; diethyl ether / 2 h / -78 °C

2: 91 percent / K₂CO₃ / methanol / 1.5 h / 20 °C

3: 83 percent / CAN / acetonitrile; H₂O / 0.33 h / 20 °C

4: 98 percent / K₂CO₃ / acetone; H₂O / 2 h / 20 °C

5: 86 percent / NaBH₄; CeCl₃*7H₂O / CH₂Cl₂; methanol / -78 - 20 °C

6: 79 percent / DABCO / W(CO)6 / tetrahydrofuran / 5 h / Heating; UV-irradiation

With 1,4-diaza-bicyclo[2.2.2]octane; sodium tetrahydroborate; cerium(III) chloride; ammonium cerium(IV) nitrate; potassium carbonate; tungsten hexacarbonyl; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; acetonitrile;
DOI:10.1021/ol7014219