o-nitrobenzenesulfenyl-p-fluorophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(γ-carboxypropyl)cysteinyl-prolyl-leucyl-glycine amide

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Chemical Name:o-nitrobenzenesulfenyl-p-fluorophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(γ-carboxypropyl)cysteinyl-prolyl-leucyl-glycine amide
CAS No.:78818-33-4
Molecular Formula:C₅₀H₇₁FN₁₂O₁₄S₂
Molecular Weight:1147.32
Hs Code.:

o-nitrobenzenesulfenyl-p-fluorophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(γ-carboxypropyl)cysteinyl-prolyl-leucyl-glycine amide

Synonyms:o-nitrobenzenesulfenyl-p-fluorophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(γ-carboxypropyl)cysteinyl-prolyl-leucyl-glycine amide

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Chemical Property of o-nitrobenzenesulfenyl-p-fluorophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(γ-carboxypropyl)cysteinyl-prolyl-leucyl-glycine amide

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Technology Process of o-nitrobenzenesulfenyl-p-fluorophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(γ-carboxypropyl)cysteinyl-prolyl-leucyl-glycine amide

There total 2 articles about o-nitrobenzenesulfenyl-p-fluorophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(γ-carboxypropyl)cysteinyl-prolyl-leucyl-glycine amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 78818-30-1
o-nitrobenzenesulfenyl-p-fluorophenylalanine pentachlorophenyl ester

: 30845-25-1
4-((R)-2-{(S)-2-[(S)-2-((2S,3S)-2-Amino-3-methyl-pentanoylamino)-4-carbamoyl-butyrylamino]-3-carbamoyl-propionylamino}-3-{(S)-2-[(S)-1-(carbamoylmethyl-carbamoyl)-3-methyl-butylcarbamoyl]-pyrrolidin-1-yl}-3-oxo-propylsulfanyl)-butyric acid

: 78818-33-4
o-nitrobenzenesulfenyl-p-fluorophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(γ-carboxypropyl)cysteinyl-prolyl-leucyl-glycine amide

Guidance literature:: With 1-ethyl-piperidine; In N,N-dimethyl-formamide; for 48h; Ambient temperature;

Reference yield:

: 78818-28-7
o-nitrobenzenesulfenyl-p-fluorophenylalanine dicyclohexylammonium salt

: 78818-33-4
o-nitrobenzenesulfenyl-p-fluorophenylalanyl-isoleucyl-glutaminyl-asparaginyl-S-(γ-carboxypropyl)cysteinyl-prolyl-leucyl-glycine amide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 1.) 0.1M-H₂SO₄ 2.)dicyclohexylcarbodiimide / 1.) ethylacetate 2.) THF

2: 89 percent / N-ethylpiperidine / dimethylformamide / 48 h / Ambient temperature

With 1-ethyl-piperidine; sulfuric acid; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;