tert-butyl 2-(2-(methoxymethoxy)-5-((4-methylpiperazin-1-yl)methyl)benzamido)-4-phenylbenzoate

Base Information

Chemical Name:tert-butyl 2-(2-(methoxymethoxy)-5-((4-methylpiperazin-1-yl)methyl)benzamido)-4-phenylbenzoate
CAS No.:1237520-11-4
Molecular Formula:C₃₂H₃₉N₃O₅
Molecular Weight:545.679
Hs Code.:

Synonyms:tert-butyl 2-(2-(methoxymethoxy)-5-((4-methylpiperazin-1-yl)methyl)benzamido)-4-phenylbenzoate

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Chemical Property of tert-butyl 2-(2-(methoxymethoxy)-5-((4-methylpiperazin-1-yl)methyl)benzamido)-4-phenylbenzoate

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Technology Process of tert-butyl 2-(2-(methoxymethoxy)-5-((4-methylpiperazin-1-yl)methyl)benzamido)-4-phenylbenzoate

There total 6 articles about tert-butyl 2-(2-(methoxymethoxy)-5-((4-methylpiperazin-1-yl)methyl)benzamido)-4-phenylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-01-3
1-methyl-piperazine

: 1237515-65-9
tert-butyl 2-(5-(bromomethyl)-2-(methoxymethoxy)benzamido)-4-phenylbenzoate

: 1237520-11-4
tert-butyl 2-(2-(methoxymethoxy)-5-((4-methylpiperazin-1-yl)methyl)benzamido)-4-phenylbenzoate

Guidance literature:: 1-methyl-piperazine; tert-butyl 2-(5-(bromomethyl)-2-(methoxymethoxy)benzamido)-4-phenylbenzoate; In acetone; at 20 ℃; for 2h; Cooling with ice;

With sodium hydroxide; In chloroform; water;

Reference yield:

: 14504-08-6
2-acetoxy-5-methylbenzoic acid

: 1237520-11-4
tert-butyl 2-(2-(methoxymethoxy)-5-((4-methylpiperazin-1-yl)methyl)benzamido)-4-phenylbenzoate

Guidance literature:: Multi-step reaction with 6 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

2: pyridine / dichloromethane / 1 h / 20 °C / Cooling with ice

3: potassium carbonate; methanol / 2.5 h / 20 °C

4: potassium carbonate / acetone / 5.83 h / 20 °C / Reflux

5: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / benzene / 0.5 h / Reflux

6: acetone / 2 h / 20 °C / Cooling with ice

With pyridine; methanol; N-Bromosuccinimide; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); potassium carbonate; N,N-dimethyl-formamide; In dichloromethane; acetone; benzene;

Reference yield:

: 1237515-64-8
tert-butyl 2-(2-hydroxy-5-methylbenzamido)-4-phenylbenzoate

: 1237520-11-4
tert-butyl 2-(2-(methoxymethoxy)-5-((4-methylpiperazin-1-yl)methyl)benzamido)-4-phenylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 5.83 h / 20 °C / Reflux

2: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / benzene / 0.5 h / Reflux

3: acetone / 2 h / 20 °C / Cooling with ice

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium carbonate; In acetone; benzene;