7-benzyloxymethyl-3,9-methano-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-15-on

Base Information

Chemical Name:7-benzyloxymethyl-3,9-methano-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-15-on
CAS No.:116171-92-7
Molecular Formula:C₂₅H₂₈N₂O₂
Molecular Weight:388.51
Hs Code.:

Synonyms:7-benzyloxymethyl-3,9-methano-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-15-on

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Chemical Property of 7-benzyloxymethyl-3,9-methano-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-15-on

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Technology Process of 7-benzyloxymethyl-3,9-methano-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-15-on

There total 9 articles about 7-benzyloxymethyl-3,9-methano-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-15-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 116171-87-0
3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeurepentafuorophenylester

: 116171-92-7
7-benzyloxymethyl-3,9-methano-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-15-on

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 40 - 50 ℃; for 1h;
DOI:10.1016/S0040-4020(01)86863-0

Reference yield:

: 107688-26-6,116260-70-9,116260-74-3
3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaurenitril

: 116171-92-7
7-benzyloxymethyl-3,9-methano-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-15-on

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / sodium hydroxide, 30percent hydrogen peroxide / ethanol / 3 h / Ambient temperature

2: 77 percent / Amberlyst 15 / 120 h / 60 °C

3: sodium hydroxide, water, ethyl acetate, HCl / ethanol / 100 h / 100 °C

4: 95 percent / dicyclohexylcarbodiimide / ethyl acetate / 15 h / Ambient temperature

5: 69 percent / H₂, / 10percent Pd/C / ethyl acetate / 1 h / 40 - 50 °C

With hydrogenchloride; sodium hydroxide; Amberlyst 15; water; hydrogen; dihydrogen peroxide; ethyl acetate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; ethyl acetate;
DOI:10.1016/S0040-4020(01)86863-0

Reference yield:

: 116171-86-9
3-benzyloxycarbonyl-7-benzyloxymethyl-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-9-carbonsaeure

: 116171-92-7
7-benzyloxymethyl-3,9-methano-1,2,3,4,5,6,7,8,9,10-decahydroazacycloundecino<5,4-b>indol-15-on

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / dicyclohexylcarbodiimide / ethyl acetate / 15 h / Ambient temperature

2: 69 percent / H₂, / 10percent Pd/C / ethyl acetate / 1 h / 40 - 50 °C

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0040-4020(01)86863-0