dimethyl (1,2-ethynediylbis(3,1-phenylene-1H-imidazote-4,2-diyl(2S)-2,1-pyrrolidinediyl((1S)-0.122-oxo-1-(tetrahydro-2H-pyran-4-yl)-2,1-ethanediyl)))biscarbamate

Base Information

Chemical Name:dimethyl (1,2-ethynediylbis(3,1-phenylene-1H-imidazote-4,2-diyl(2S)-2,1-pyrrolidinediyl((1S)-0.122-oxo-1-(tetrahydro-2H-pyran-4-yl)-2,1-ethanediyl)))biscarbamate
CAS No.:1250941-34-4
Molecular Formula:C₄₆H₅₄N₈O₈
Molecular Weight:846.984
Hs Code.:

dimethyl (1,2-ethynediylbis(3,1-phenylene-1H-imidazote-4,2-diyl(2S)-2,1-pyrrolidinediyl((1S)-0.122-oxo-1-(tetrahydro-2H-pyran-4-yl)-2,1-ethanediyl)))biscarbamate

Synonyms:dimethyl (1,2-ethynediylbis(3,1-phenylene-1H-imidazote-4,2-diyl(2S)-2,1-pyrrolidinediyl((1S)-0.122-oxo-1-(tetrahydro-2H-pyran-4-yl)-2,1-ethanediyl)))biscarbamate

Suppliers and Price of dimethyl (1,2-ethynediylbis(3,1-phenylene-1H-imidazote-4,2-diyl(2S)-2,1-pyrrolidinediyl((1S)-0.122-oxo-1-(tetrahydro-2H-pyran-4-yl)-2,1-ethanediyl)))biscarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dimethyl (1,2-ethynediylbis(3,1-phenylene-1H-imidazote-4,2-diyl(2S)-2,1-pyrrolidinediyl((1S)-0.122-oxo-1-(tetrahydro-2H-pyran-4-yl)-2,1-ethanediyl)))biscarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dimethyl (1,2-ethynediylbis(3,1-phenylene-1H-imidazote-4,2-diyl(2S)-2,1-pyrrolidinediyl((1S)-0.122-oxo-1-(tetrahydro-2H-pyran-4-yl)-2,1-ethanediyl)))biscarbamate

There total 7 articles about dimethyl (1,2-ethynediylbis(3,1-phenylene-1H-imidazote-4,2-diyl(2S)-2,1-pyrrolidinediyl((1S)-0.122-oxo-1-(tetrahydro-2H-pyran-4-yl)-2,1-ethanediyl)))biscarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1009120-03-9
(S)-methoxycarbonylamino(tetrahydropyran-4-yl)acetic acid

: (x)C₂HF₃O₂*C₂₈H₂₈N₆

: 1250941-34-4
dimethyl (1,2-ethynediylbis(3,1-phenylene-1H-imidazote-4,2-diyl(2S)-2,1-pyrrolidinediyl((1S)-0.122-oxo-1-(tetrahydro-2H-pyran-4-yl)-2,1-ethanediyl)))biscarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 1007882-08-7
C₁₈H₂₂BrN₃O₂

: 1250941-34-4
dimethyl (1,2-ethynediylbis(3,1-phenylene-1H-imidazote-4,2-diyl(2S)-2,1-pyrrolidinediyl((1S)-0.122-oxo-1-(tetrahydro-2H-pyran-4-yl)-2,1-ethanediyl)))biscarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 90 °C / Inert atmosphere

2: 1,2-dichloro-ethane / 1 h / 20 °C

3: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 2 h / 20 °C

With N-ethyl-N,N-diisopropylamine; HATU; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 1208008-33-6
(3S)-tert-butyl 3-(tert-butyldiphenylsiloxymethyl)-2-azabicyclo[3.1.0]hexane-2-carboxylate

: 1250941-34-4
dimethyl (1,2-ethynediylbis(3,1-phenylene-1H-imidazote-4,2-diyl(2S)-2,1-pyrrolidinediyl((1S)-0.122-oxo-1-(tetrahydro-2H-pyran-4-yl)-2,1-ethanediyl)))biscarbamate

Guidance literature:: Multi-step reaction with 7 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

2: sodium periodate / ruthenium trichloride / tetrachloromethane; water; acetonitrile / 1.25 h

3: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C

4: ammonium acetate / xylene / 140 °C / Sealed tube; Inert atmosphere

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 90 °C / Inert atmosphere

6: 1,2-dichloro-ethane / 1 h / 20 °C

7: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 2 h / 20 °C

With sodium periodate; ammonium acetate; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; HATU; ruthenium trichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; tetrachloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; xylene;