Butanedioic acid, 2-bromo-3-hydroxy-, dimethyl ester, (2R,3S)-rel- (9CI)

Base Information

Chemical Name:Butanedioic acid, 2-bromo-3-hydroxy-, dimethyl ester, (2R,3S)-rel- (9CI)
CAS No.:256530-26-4
Molecular Formula:C₆H₉BrO₅
Molecular Weight:241.038
Hs Code.:
Mol file:256530-26-4.mol

Synonyms:Butanedioicacid, 2-bromo-3-hydroxy-, dimethyl ester, (2R,3S)-rel- (9CI)

Suppliers and Price of Butanedioic acid, 2-bromo-3-hydroxy-, dimethyl ester, (2R,3S)-rel- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Butanedioic acid, 2-bromo-3-hydroxy-, dimethyl ester, (2R,3S)-rel- (9CI)

Chemical Property:

PSA：72.83000
LogP:-0.54320

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Butanedioic acid, 2-bromo-3-hydroxy-, dimethyl ester, (2R,3S)-rel- (9CI)

There total 6 articles about Butanedioic acid, 2-bromo-3-hydroxy-, dimethyl ester, (2R,3S)-rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 78816-00-9
dimethyl (2R)-acetoxy-(3S)-bromosuccinate

: 109874-90-0,256530-26-4
dimethyl (2S,3R)-2-bromo-3-hydroxysuccinate

Guidance literature:: With hydrogenchloride; In methanol; at 22 ℃; for 46h;
DOI:10.1021/ja00350a059

Reference yield: 75.0%

: 13171-64-7
Dimethyl D-tartrate

: 749917-66-6,256530-26-4
dimethyl (2R,3R)-2-bromo-3-hydroxysuccinate

Guidance literature:: With hydrogen bromide; In acetic acid;

Reference yield:

: 608-68-4
dimethyl L-tartrate

: 109874-90-0,256530-26-4
dimethyl (2S,3R)-2-bromo-3-hydroxysuccinate

Guidance literature:: With methanol; hydrogen bromide; acetic acid; acetyl chloride; Yield given. Multistep reaction; 1) r.t., 10 h, 2) reflux, 6 h;
DOI:10.1016/S0040-4020(01)92187-8