C₃₆H₃₃N₃

Base Information

Chemical Name:C₃₆H₃₃N₃
CAS No.:1058114-75-2
Molecular Formula:C₃₆H₃₃N₃
Molecular Weight:507.678
Hs Code.:

C<sub>36</sub>H<sub>33</sub>N<sub>3</sub>

Synonyms:C₃₆H₃₃N₃

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Chemical Property of C₃₆H₃₃N₃

Chemical Property:

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Technology Process of C₃₆H₃₃N₃

There total 5 articles about C₃₆H₃₃N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1058114-19-4
C₃₆H₃₁N₃O

: 1058114-75-2
C₃₆H₃₃N₃

Guidance literature:: C₃₆H₃₁N₃O; With dimethylsulfide borane complex; In tetrahydrofuran; for 1h; Heating / reflux;

With ethanol; for 0.5h; Heating / reflux;

Reference yield:

: 1590-24-5
(7-bromo-1-naphthalenyl)ethanone

: 1058114-75-2
C₃₆H₃₃N₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 100 °C

2.1: ethylmagnesium bromide / diethyl ether; dichloromethane / 0.75 h / 0 - 20 °C

2.2: 1.5 h / 0 - 20 °C

2.3: 0 °C

3.1: dimethylsilicon dichloride; sodium iodide / dichloromethane; acetonitrile / 0.5 h

4.1: hydroxylamine hydrochloride; sodium acetate / methanol / 20 °C

5.1: triethylamine / tetrahydrofuran / 0.5 h / 20 °C

6.1: dimethylsulfide borane complex / tetrahydrofuran / 1 h / Heating / reflux

6.2: 0.5 h / Heating / reflux

With dimethylsulfide borane complex; ethylmagnesium bromide; hydroxylamine hydrochloride; sodium acetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; dimethylsilicon dichloride; sodium iodide; palladium diacetate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; acetonitrile;

Reference yield:

: 580-13-2
2-bromonaphthalene

: 1058114-75-2
C₃₆H₃₃N₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: aluminum (III) chloride / dichloromethane / 5 h / -78 °C

2.1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 100 °C

3.1: ethylmagnesium bromide / diethyl ether; dichloromethane / 0.75 h / 0 - 20 °C

3.2: 1.5 h / 0 - 20 °C

3.3: 0 °C

4.1: dimethylsilicon dichloride; sodium iodide / dichloromethane; acetonitrile / 0.5 h

5.1: hydroxylamine hydrochloride; sodium acetate / methanol / 20 °C

6.1: triethylamine / tetrahydrofuran / 0.5 h / 20 °C

7.1: dimethylsulfide borane complex / tetrahydrofuran / 1 h / Heating / reflux

7.2: 0.5 h / Heating / reflux

With aluminum (III) chloride; dimethylsulfide borane complex; ethylmagnesium bromide; hydroxylamine hydrochloride; sodium acetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; dimethylsilicon dichloride; sodium iodide; palladium diacetate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; acetonitrile;