1,2,3,4-tetrahydro-4-phenylsulphonylpyrrolo<1',2':1,2>-pyrrolo<3,4-b>indole

Base Information

• Chemical Name: 1,2,3,4-tetrahydro-4-phenylsulphonylpyrrolo<1',2':1,2>-pyrrolo<3,4-b>indole
• CAS No.: 112565-53-4
• Molecular Formula: C₁₉H₁₆N₂O₂S
• Molecular Weight: 336.414

Synonyms:1,2,3,4-tetrahydro-4-phenylsulphonylpyrrolo<1',2':1,2>-pyrrolo<3,4-b>indole

Chemical Property of 1,2,3,4-tetrahydro-4-phenylsulphonylpyrrolo<1',2':1,2>-pyrrolo<3,4-b>indole

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Technology Process of 1,2,3,4-tetrahydro-4-phenylsulphonylpyrrolo<1',2':1,2>-pyrrolo<3,4-b>indole

There total 9 articles about 1,2,3,4-tetrahydro-4-phenylsulphonylpyrrolo<1',2':1,2>-pyrrolo<3,4-b>indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

7-Benzenesulfonyl-6-oxo-1,3,4,5,6,7-hexahydro-azocino[4,3-b]indole-2-carboxylic acid benzyl ester (112565-50-1) → 1,2,3,4-tetrahydro-4-phenylsulphonylpyrrolo<1',2':1,2>-pyrrolo<3,4-b>indole (112565-53-4)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 0.5h; Ambient temperature;

DOI:10.1039/P19870001599

Reference yield: 74.0%

1,2,3,4-tetrahydro-2-phenoxycarbonyl-7-phenylsulphonylazocino<4,3-b>indol-6 (5H)-one (112565-51-2) → 1,2,3,4-tetrahydro-4-phenylsulphonylpyrrolo<1',2':1,2>-pyrrolo<3,4-b>indole (112565-53-4)

Guidance literature:

With methyllithium lithium bromide; diethyl ether; In tetrahydrofuran; at 0 ℃; for 2.5h;

DOI:10.1039/P19870001599

Reference yield: 69.0%

7-Benzenesulfonyl-6-oxo-1,3,4,5,6,7-hexahydro-azocino[4,3-b]indole-2-carboxylic acid 9H-fluoren-9-ylmethyl ester (112565-52-3) → 1,2,3,4-tetrahydro-4-phenylsulphonylpyrrolo<1',2':1,2>-pyrrolo<3,4-b>indole (112565-53-4)

Guidance literature:

With piperidine; for 1.5h; Ambient temperature;

DOI:10.1039/P19870001599

upstream raw materials:

1,2,3,4-tetrahydro-2-phenoxycarbonyl-7-phenylsulphonylazocino<4,3-b>indol-6 (5H)-one

7-Benzenesulfonyl-6-oxo-1,3,4,5,6,7-hexahydro-azocino[4,3-b]indole-2-carboxylic acid benzyl ester

7-Benzenesulfonyl-6-oxo-1,3,4,5,6,7-hexahydro-azocino[4,3-b]indole-2-carboxylic acid 9H-fluoren-9-ylmethyl ester

1-benzenesulfonylindole

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