C₁₃H₁₃N₃O₃

Base Information

Chemical Name:C₁₃H₁₃N₃O₃
CAS No.:1429195-15-2
Molecular Formula:C₁₃H₁₃N₃O₃
Molecular Weight:259.265
Hs Code.:

C<sub>13</sub>H<sub>13</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₁₃H₁₃N₃O₃

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Chemical Property of C₁₃H₁₃N₃O₃

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Technology Process of C₁₃H₁₃N₃O₃

There total 5 articles about C₁₃H₁₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1429195-14-1
C₁₆H₁₉N₃O₄

: 1429195-15-2
C₁₃H₁₃N₃O₃

Guidance literature:: With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; In 1,4-dioxane; water; isopropyl alcohol; at 20 ℃; for 6h;
DOI:10.1016/j.tet.2013.03.057

Reference yield:

: 1429195-13-0
(1S,2S,3R)-1-azido-1-phenylhex-5-ene-2,3-diol

: 1429195-15-2
C₁₃H₁₃N₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dmap / 3 h / 20 °C / Inert atmosphere

2: sodium periodate; 2,6-dimethylpyridine; osmium(VIII) oxide / 1,4-dioxane; water; isopropyl alcohol / 6 h / 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; sodium periodate; osmium(VIII) oxide; In 1,4-dioxane; water; isopropyl alcohol;
DOI:10.1016/j.tet.2013.03.057

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 1429195-15-2
C₁₃H₁₃N₃O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran / 2.75 h / 0 - 20 °C

2.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 0.25 h / -20 °C

2.2: 3 h / -20 °C / Molecular sieve

3.1: sodium azide / acetonitrile / Molecular sieve

4.1: pyridine; dmap / 3 h / 20 °C / Inert atmosphere

5.1: sodium periodate; 2,6-dimethylpyridine; osmium(VIII) oxide / 1,4-dioxane; water; isopropyl alcohol / 6 h / 20 °C

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; dmap; sodium periodate; osmium(VIII) oxide; sodium azide; diethyl (2S,3S)-tartrate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; isopropyl alcohol; acetonitrile;
DOI:10.1016/j.tet.2013.03.057