p-tolyl thioclavulanate

Base Information

Chemical Name:p-tolyl thioclavulanate
CAS No.:91022-05-8
Molecular Formula:C₁₅H₁₅NO₄S
Molecular Weight:305.354
Hs Code.:

Synonyms:p-tolyl thioclavulanate

Suppliers and Price of p-tolyl thioclavulanate

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Chemical Property of p-tolyl thioclavulanate

Chemical Property:

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Technology Process of p-tolyl thioclavulanate

There total 3 articles about p-tolyl thioclavulanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57943-82-5
methyl clavulanate

: 91022-05-8
p-tolyl thioclavulanate

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / sodium hydroxide / H₂O / 1.17 h / 0 °C

2: 69 percent / dimethylformamide / 1.5 h / Ambient temperature

3: 84 percent / H₂ / palladium on carbon / ethanol / 0.75 h / 760 Torr / Ambient temperature

4: 17 percent / dicyclohexylcarbodi-imide / acetonitrile / Ambient temperature

With sodium hydroxide; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 57943-81-4
potassium clavulanate

: 91022-05-8
p-tolyl thioclavulanate

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / dimethylformamide / 1.5 h / Ambient temperature

2: 84 percent / H₂ / palladium on carbon / ethanol / 0.75 h / 760 Torr / Ambient temperature

3: 17 percent / dicyclohexylcarbodi-imide / acetonitrile / Ambient temperature

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 57943-84-7
Benzyl Clavulanate

: 91022-05-8
p-tolyl thioclavulanate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / H₂ / palladium on carbon / ethanol / 0.75 h / 760 Torr / Ambient temperature

2: 17 percent / dicyclohexylcarbodi-imide / acetonitrile / Ambient temperature

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; acetonitrile;