5,12-bis(3,5-di-tert-butylphenoxy)-2-octyl-5a,14c-dihydroanthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Base Information

• Chemical Name: 5,12-bis(3,5-di-tert-butylphenoxy)-2-octyl-5a,14c-dihydroanthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone
• CAS No.: 848077-92-9
• Molecular Formula: C₆₀H₆₆N₂O₆
• Molecular Weight: 911.194

Synonyms:5,12-bis(3,5-di-tert-butylphenoxy)-2-octyl-5a,14c-dihydroanthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Chemical Property of 5,12-bis(3,5-di-tert-butylphenoxy)-2-octyl-5a,14c-dihydroanthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 5,12-bis(3,5-di-tert-butylphenoxy)-2-octyl-5a,14c-dihydroanthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

There total 1 articles about 5,12-bis(3,5-di-tert-butylphenoxy)-2-octyl-5a,14c-dihydroanthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-(2-ethylhexyl)-1,7-(3',5'-di-tert-butoxyphenoxy)perylene-3,4-dicarboxyanydride-9,10-dicarboxyimide → 5,12-bis(3,5-di-tert-butylphenoxy)-2-octyl-5a,14c-dihydroanthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone (848077-92-9)

Guidance literature:

With urea; In N,N-dimethyl-formamide; Heating;

DOI:10.1021/jo0481351

Reference yield: 74.0%

5,12-bis(3,5-di-tert-butylphenoxy)-2-octyl-5a,14c-dihydroanthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone (848077-92-9) + 2-Phenyl-1,3,2-dioxaborinane (4406-77-3) → 5,12-bis(3,5-di-tert-butylphenoxy)-2-octyl-9-phenyl-5a,14c-dihydroanthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Guidance literature:

With copper diacetate; oxygen; triethylamine; 4 A molecular sieve; In chloroform; at 40 ℃; for 48h;

DOI:10.1021/jo0481351

Reference yield: 73.0%

5,12-bis(3,5-di-tert-butylphenoxy)-2-octyl-5a,14c-dihydroanthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone (848077-92-9) + 4-(1,3,2-dioxaborinan-2-yl)-benzaldehyde → 4-[6,13-bis(3,5-di-tert-butylphenoxy)-9-octyl-1,3,8,10-tetraoxo-3,5b,8,9,10,10c-hexahydro-1H-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinolin-2-yl]benzaldehyde

Guidance literature:

With copper diacetate; oxygen; triethylamine; 4 A molecular sieve; In chloroform; at 40 ℃; for 48h;

DOI:10.1021/jo0481351

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