1-[3-{4-(3-morpholinopropoxy)phenyl}-3-hydroxypropyl]-3-isopropylthiourea

Base Information

Chemical Name:1-[3-{4-(3-morpholinopropoxy)phenyl}-3-hydroxypropyl]-3-isopropylthiourea
CAS No.:1467720-03-1
Molecular Formula:C₂₀H₃₃N₃O₃S
Molecular Weight:395.566
Hs Code.:

Synonyms:1-[3-{4-(3-morpholinopropoxy)phenyl}-3-hydroxypropyl]-3-isopropylthiourea

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Chemical Property of 1-[3-{4-(3-morpholinopropoxy)phenyl}-3-hydroxypropyl]-3-isopropylthiourea

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Technology Process of 1-[3-{4-(3-morpholinopropoxy)phenyl}-3-hydroxypropyl]-3-isopropylthiourea

There total 10 articles about 1-[3-{4-(3-morpholinopropoxy)phenyl}-3-hydroxypropyl]-3-isopropylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2253-73-8
isopropyl isothiocyanate

: 1-(4-(3-morpholinopropoxy)phenyl)-3-aminopropan-1-ol

: 1467720-03-1
1-[3-{4-(3-morpholinopropoxy)phenyl}-3-hydroxypropyl]-3-isopropylthiourea

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 24h;

Reference yield: 93.0%

: 1719-76-2
1-isopropylthiourea

: 1-(4-(3-morpholinopropoxy)phenyl)-3-aminopropan-1-ol

: 1467720-03-1
1-[3-{4-(3-morpholinopropoxy)phenyl}-3-hydroxypropyl]-3-isopropylthiourea

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.5012/bkcs.2013.34.8.2317

Reference yield:

: 1-(4-(3-morpholinopropoxy)phenyl)-3-azidopropan-1-ol

: 1467720-03-1
1-[3-{4-(3-morpholinopropoxy)phenyl}-3-hydroxypropyl]-3-isopropylthiourea

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 1 h / 0 - 20 °C

2: dichloromethane / 12 h / 0 - 20 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.5012/bkcs.2013.34.8.2317